benzyloxycarbonylalanyl-glycine hydrazide

Base Information

Chemical Name:benzyloxycarbonylalanyl-glycine hydrazide
CAS No.:58651-28-8
Molecular Formula:C₁₃H₁₈N₄O₄
Molecular Weight:294.31
Hs Code.:

Synonyms:benzyloxycarbonylalanyl-glycine hydrazide

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Chemical Property of benzyloxycarbonylalanyl-glycine hydrazide

Chemical Property:

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Technology Process of benzyloxycarbonylalanyl-glycine hydrazide

There total 7 articles about benzyloxycarbonylalanyl-glycine hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 2503-32-4
ethyl N-(benzyloxycarbonyl)-L-alanylglycinate

: 58651-28-8
benzyloxycarbonylalanyl-glycine hydrazide

Guidance literature:: With hydrazine hydrate; In methanol; for 24h; Ambient temperature;

Reference yield:

: 1142-20-7
N-Cbz-Ala

: 58651-28-8
benzyloxycarbonylalanyl-glycine hydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: 67 percent / SOCl₂; Et₃N / toluene / 2 h / 5 °C

2: 59 percent / Et₃N / tetrahydrofuran / 1.33 h / Heating

3: hydrazine hydrate / methanol / 1.33 h / Heating

With thionyl chloride; hydrazine hydrate; triethylamine; In tetrahydrofuran; methanol; toluene; 1: Substitution / 2: Substitution / 3: Substitution;
DOI:10.3987/COM-99-S51

Reference yield:

: 28819-05-8
(S)-2-benzyloxycarbonylamino-propionic acid methyl ester

: 58651-28-8
benzyloxycarbonylalanyl-glycine hydrazide

Guidance literature:: Multi-step reaction with 4 steps

1: hydrazine hydrate / methanol / 1.33 h / Heating

2: p-toluenesulfonic acid / methanol / 16 h / 20 °C

3: 59 percent / Et₃N / tetrahydrofuran / 1.33 h / Heating

4: hydrazine hydrate / methanol / 1.33 h / Heating

With toluene-4-sulfonic acid; hydrazine hydrate; triethylamine; In tetrahydrofuran; methanol; 1: Substitution / 2: cyclocondensation / 3: Substitution / 4: Substitution;
DOI:10.3987/COM-99-S51