N--N'-t-butylhydrazine

Base Information

Chemical Name:N--N'-t-butylhydrazine
CAS No.:105077-58-5
Molecular Formula:C₁₆H₁₉Cl₂N₂O₃P
Molecular Weight:389.218
Hs Code.:

N-<bis(p-chlorophenoxy)phosphinoyl>-N'-t-butylhydrazine

Synonyms:N--N'-t-butylhydrazine

Suppliers and Price of N--N'-t-butylhydrazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N--N'-t-butylhydrazine

Chemical Property:

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Technology Process of N--N'-t-butylhydrazine

There total 3 articles about N--N'-t-butylhydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 15074-53-0
bis(4-chlorophenyl)phosphoryl chloride

: 7400-27-3
tertbutylhydrazine hydrochloride

: 105077-58-5
N--N'-t-butylhydrazine

Guidance literature:: With triethylamine; In dichloromethane; for 0.5h; Ambient temperature;

Reference yield:

: 15074-53-0
bis(4-chlorophenyl)phosphoryl chloride

: 105077-58-5
N--N'-t-butylhydrazine

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) O-trimethylsilylhydroxylamine, pyridine, 2.) methanol / 1.) dichloromethane, r.t., 2.5 h, 2.) 15 min

2: 1.) pyridine, 2.) aq. HCl / 1.) 0 deg C, 5.5 min, 2.) chloroform

3: 1 h / Ambient temperature

With pyridine; hydrogenchloride; methanol; O-Trimethylsilylhydroxylamine;