3,4,9,10-tetraphenyl-1,2,5,6,8,11-hexaazacyclododeca-7,12-dithione-2,4,8,10-tetraene

Base Information

Chemical Name:3,4,9,10-tetraphenyl-1,2,5,6,8,11-hexaazacyclododeca-7,12-dithione-2,4,8,10-tetraene
CAS No.:213821-73-9
Molecular Formula:C₃₀H₂₂N₆S₂
Molecular Weight:530.677
Hs Code.:

Synonyms:3,4,9,10-tetraphenyl-1,2,5,6,8,11-hexaazacyclododeca-7,12-dithione-2,4,8,10-tetraene

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Chemical Property of 3,4,9,10-tetraphenyl-1,2,5,6,8,11-hexaazacyclododeca-7,12-dithione-2,4,8,10-tetraene

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Technology Process of 3,4,9,10-tetraphenyl-1,2,5,6,8,11-hexaazacyclododeca-7,12-dithione-2,4,8,10-tetraene

There total 2 articles about 3,4,9,10-tetraphenyl-1,2,5,6,8,11-hexaazacyclododeca-7,12-dithione-2,4,8,10-tetraene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 30131-95-4
5,6-diphenyl-2,3,4,5-tetrahydro-5-ethoxy-1,2,4-triazine-3-thione

: 213821-73-9
3,4,9,10-tetraphenyl-1,2,5,6,8,11-hexaazacyclododeca-7,12-dithione-2,4,8,10-tetraene

Guidance literature:: With chromium chloride; In ethanol; at 20 ℃;

Reference yield:

: 134-81-6
benzil

: 213821-73-9
3,4,9,10-tetraphenyl-1,2,5,6,8,11-hexaazacyclododeca-7,12-dithione-2,4,8,10-tetraene

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / 2M aq. HCl / 8 h / Heating

2: 68 percent / CrCl₃*6H₂O / ethanol / 20 °C

With hydrogenchloride; chromium chloride; In ethanol;

Reference yield: 60.0%

: 142-71-2
copper diacetate

: 213821-73-9
3,4,9,10-tetraphenyl-1,2,5,6,8,11-hexaazacyclododeca-7,12-dithione-2,4,8,10-tetraene

: 475560-41-9,274918-96-6
Cu(3,4,9,10-tetraphenyl-1,2,5,6,8,11-hexaazacyclododeca-7,12-dithione-2,4,8,10-tetraene^(2-))

Guidance literature:: In ethanol; ethanolic soln. of metal salt added to warm ethanolic suspn. of ligand, heated under reflux with stirring for 2 h; cooling, ppt. filtered off, washed with ethanol, dried over P4O10; elem.anal.;