C₂₇H₂₉N₃O₄S

Base Information

Chemical Name:C₂₇H₂₉N₃O₄S
CAS No.:1177423-70-9
Molecular Formula:C₂₇H₂₉N₃O₄S
Molecular Weight:491.611
Hs Code.:

C<sub>27</sub>H<sub>29</sub>N<sub>3</sub>O<sub>4</sub>S

Synonyms:C₂₇H₂₉N₃O₄S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₇H₂₉N₃O₄S

Chemical Property:

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Technology Process of C₂₇H₂₉N₃O₄S

There total 9 articles about C₂₇H₂₉N₃O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₈H₃₁N₃O₄S

: 1177423-70-9
C₂₇H₂₉N₃O₄S

Guidance literature:: With hydrogenchloride; water; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield:

: 1008119-10-5
(E)-4-(3-(dimethylamino)acryloyl)-N,N-dimethylbenzamide

: 1177423-70-9
C₂₇H₂₉N₃O₄S

Guidance literature:: Multi-step reaction with 5 steps

1.1: acetic acid / N,N-dimethyl acetamide / 6.5 h / 120 °C / Inert atmosphere

2.1: sodium tetrahydroborate / methanol; dichloromethane / 1 h / 0 °C

3.1: titanium tetrachloride / dichloromethane / 0.5 h / 0 °C

3.2: 1 h / 0 °C

4.1: sodium isopropanethiolate / N,N-dimethyl-formamide / 1 h / 50 °C

5.1: hydrogenchloride; water / N,N-dimethyl-formamide / 20 °C

With hydrogenchloride; sodium tetrahydroborate; water; sodium isopropanethiolate; titanium tetrachloride; acetic acid; In methanol; dichloromethane; N,N-dimethyl acetamide; N,N-dimethyl-formamide;

Reference yield:

: 586-89-0
4-acetyl-benzoic acid

: 1177423-70-9
C₂₇H₂₉N₃O₄S

Guidance literature:: Multi-step reaction with 7 steps

1.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / water; acetonitrile / 15 h / 20 °C

2.1: 15 h / Heating; Reflux

3.1: acetic acid / N,N-dimethyl acetamide / 6.5 h / 120 °C / Inert atmosphere

4.1: sodium tetrahydroborate / methanol; dichloromethane / 1 h / 0 °C

5.1: titanium tetrachloride / dichloromethane / 0.5 h / 0 °C

5.2: 1 h / 0 °C

6.1: sodium isopropanethiolate / N,N-dimethyl-formamide / 1 h / 50 °C

7.1: hydrogenchloride; water / N,N-dimethyl-formamide / 20 °C

With hydrogenchloride; sodium tetrahydroborate; water; sodium isopropanethiolate; titanium tetrachloride; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane; N,N-dimethyl acetamide; water; N,N-dimethyl-formamide; acetonitrile;