4-((5-(4-(bis(4-methoxybenzyl)amino)-6-methyl-1,3,5-triazin-2-yl)-6-((6-methoxypyridin-3-yl)amino)pyridin-3-yl)methyl)-thiomorpholine 1,1-dioxide

Base Information

Chemical Name:4-((5-(4-(bis(4-methoxybenzyl)amino)-6-methyl-1,3,5-triazin-2-yl)-6-((6-methoxypyridin-3-yl)amino)pyridin-3-yl)methyl)-thiomorpholine 1,1-dioxide
CAS No.:1379860-80-6
Molecular Formula:C₃₆H₄₀N₈O₅S
Molecular Weight:696.83
Hs Code.:

Synonyms:4-((5-(4-(bis(4-methoxybenzyl)amino)-6-methyl-1,3,5-triazin-2-yl)-6-((6-methoxypyridin-3-yl)amino)pyridin-3-yl)methyl)-thiomorpholine 1,1-dioxide

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Chemical Property of 4-((5-(4-(bis(4-methoxybenzyl)amino)-6-methyl-1,3,5-triazin-2-yl)-6-((6-methoxypyridin-3-yl)amino)pyridin-3-yl)methyl)-thiomorpholine 1,1-dioxide

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Technology Process of 4-((5-(4-(bis(4-methoxybenzyl)amino)-6-methyl-1,3,5-triazin-2-yl)-6-((6-methoxypyridin-3-yl)amino)pyridin-3-yl)methyl)-thiomorpholine 1,1-dioxide

There total 4 articles about 4-((5-(4-(bis(4-methoxybenzyl)amino)-6-methyl-1,3,5-triazin-2-yl)-6-((6-methoxypyridin-3-yl)amino)pyridin-3-yl)methyl)-thiomorpholine 1,1-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 39093-93-1
thiomorpholine 1,1-dioxide

: 1253574-95-6
(5-(4-(bis(4-methoxybenzyl)amino)-6-methyl-1,3,5-triazin-2-yl)-6-(6-methoxypyridin-3-ylamino)pyridin-3-yl)methyl methanesulfonate

: 1379860-80-6
4-((5-(4-(bis(4-methoxybenzyl)amino)-6-methyl-1,3,5-triazin-2-yl)-6-((6-methoxypyridin-3-yl)amino)pyridin-3-yl)methyl)-thiomorpholine 1,1-dioxide

Guidance literature:: With triethylamine; In tetrahydrofuran; at 80 ℃; for 4h; Inert atmosphere;
DOI:10.1021/jm300184s

Reference yield:

: 1253571-12-8
4-(5-(1,3-dioxolan-2-yl)-2-fluoropyridin-3-yl)-N,N-bis-(4-methoxybenzyl)-6-methyl-1,3,5-triazin-2-amine

: 1379860-80-6
4-((5-(4-(bis(4-methoxybenzyl)amino)-6-methyl-1,3,5-triazin-2-yl)-6-((6-methoxypyridin-3-yl)amino)pyridin-3-yl)methyl)-thiomorpholine 1,1-dioxide

Guidance literature:: Multi-step reaction with 4 steps

1: lithium hexamethyldisilazane / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

2: sodium tetrahydroborate / methanol / 0.83 h / 0 - 22 °C / Inert atmosphere

3: triethylamine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

4: triethylamine / tetrahydrofuran / 4 h / 80 °C / Inert atmosphere

With sodium tetrahydroborate; triethylamine; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jm300184s

Reference yield:

: 1253571-18-4
5-(4-(bis(4-methoxybenzyl)amino)-6-methyl-1,3,5-triazin-2-yl)-6-(6-methoxypyridin-3-ylamino)nicotinaldehyde

: 1379860-80-6
4-((5-(4-(bis(4-methoxybenzyl)amino)-6-methyl-1,3,5-triazin-2-yl)-6-((6-methoxypyridin-3-yl)amino)pyridin-3-yl)methyl)-thiomorpholine 1,1-dioxide

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tetrahydroborate / methanol / 0.83 h / 0 - 22 °C / Inert atmosphere

2: triethylamine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

3: triethylamine / tetrahydrofuran / 4 h / 80 °C / Inert atmosphere

With sodium tetrahydroborate; triethylamine; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jm300184s