C₆₉H₉₄N₂O₁₆Si

Base Information

Chemical Name:C₆₉H₉₄N₂O₁₆Si
CAS No.:245736-69-0
Molecular Formula:C₆₉H₉₄N₂O₁₆Si
Molecular Weight:1235.59
Hs Code.:

C<sub>69</sub>H<sub>94</sub>N<sub>2</sub>O<sub>16</sub>Si

Synonyms:C₆₉H₉₄N₂O₁₆Si

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Chemical Property of C₆₉H₉₄N₂O₁₆Si

Chemical Property:

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Technology Process of C₆₉H₉₄N₂O₁₆Si

There total 37 articles about C₆₉H₉₄N₂O₁₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 69739-34-0
t-butyldimethylsiyl triflate

: 245736-69-0
C₆₉H₉₄N₂O₁₆Si

Guidance literature:: Multi-step reaction with 8 steps

1: 1.) 2,6-lutidine, 2.) KO-t-Bu / 1.) CH₂Cl₂, -78 deg C, 2.) THF, -10 deg C

2: DIBAL-H / tetrahydrofuran / -78 - 23 °C

3: Br₂, Ph₃P, imidazole, 2-methyl-2-butene / CH₂Cl₂

4: 78 percent / AgNO₂ / diethyl ether

5: 1.) 3-ClPhNCO, i-Pr₂NEt / 1.) PhMe, 2.) PhMe, 90 deg C

6: PPTS / methanol / 0 °C

7: SO₃*pyr, i-Pr₂NEt / dimethylsulfoxide; CH₂Cl₂ / -15 °C

8: 1.) c-hex2BCl, Me₂NEt / 1.) Et₂O, 0 deg C, 2.) Et₂O, from -78 deg C to 0 deg C

With 1H-imidazole; 2,6-dimethylpyridine; silver(I) nitrite; 2-methyl-but-2-ene; pyridine-SO₃ complex; N,N-dimethyl-ethanamine; dicyclohexylboron chloride; potassium tert-butylate; bromine; pyridinium p-toluenesulfonate; diisobutylaluminium hydride; N-ethyl-N,N-diisopropylamine; triphenylphosphine; m-chlorophenyl isocyanate; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; dimethyl sulfoxide;
DOI:10.1021/ja990789h

Reference yield:

: 100-39-0
benzyl bromide

: 245736-69-0
C₆₉H₉₄N₂O₁₆Si

Guidance literature:: Multi-step reaction with 4 steps

1: Cs₂CO₃ / dimethylformamide; CH₂Cl₂

2: aq. OsO₄, NMO / tetrahydrofuran; 2-methyl-propan-2-ol

3: aq. NaIO₄, NaHCO₃ / tetrahydrofuran; 2-methyl-propan-2-ol

4: 1.) c-hex2BCl, Me₂NEt / 1.) Et₂O, 0 deg C, 2.) Et₂O, from -78 deg C to 0 deg C

With sodium periodate; osmium(VIII) oxide; N-methyl-2-indolinone; N,N-dimethyl-ethanamine; dicyclohexylboron chloride; sodium hydrogencarbonate; caesium carbonate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1021/ja990789h

Reference yield:

: 2746-25-0
p-Methoxybenzyl bromide

: 245736-69-0
C₆₉H₉₄N₂O₁₆Si

Guidance literature:: Multi-step reaction with 17 steps

1: NaH / dimethylformamide; tetrahydrofuran

2: HCl / methanol; diethyl ether / 0 °C

3: (COCl)2, DMSO, i-Pr₂NEt / -78 - -30 °C

4: 73 percent / TiCl₂(O-i-Pr)2 / CH₂Cl₂ / -78 - 0 °C

5: Et₂BOMe, NaBH₄ / tetrahydrofuran; methanol / -78 °C

6: HCl

7: DIBAL-H / CH₂Cl₂ / -78 °C

8: 1.) Bu₂BOTf, i-Pr₂NEt / 1.) CH₂Cl₂, 0 deg C, 2.) CH₂Cl₂, -78 deg C

9: 100 percent / (COCl)2, DMSO, i-Pr₂NEt / -78 - 0 °C

10: 82 percent / TsOH / acetonitrile / -22 °C

11: 100 percent / (COCl)2, DMSO, Et₃N / -78 - 0 °C

12: LDA / 1 h / -78 °C

13: LiOOH / tetrahydrofuran; dimethylformamide; H₂O / 0 - 23 °C

14: Cs₂CO₃ / dimethylformamide; CH₂Cl₂

15: aq. OsO₄, NMO / tetrahydrofuran; 2-methyl-propan-2-ol

16: aq. NaIO₄, NaHCO₃ / tetrahydrofuran; 2-methyl-propan-2-ol

17: 1.) c-hex2BCl, Me₂NEt / 1.) Et₂O, 0 deg C, 2.) Et₂O, from -78 deg C to 0 deg C

With hydrogenchloride; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; N-methyl-2-indolinone; titanium(IV) dichlorodiisopropylate; oxalyl dichloride; lithium hydroperoxide; N,N-dimethyl-ethanamine; di-n-butylboryl trifluoromethanesulfonate; diethyl methoxy borane; dicyclohexylboron chloride; sodium hydride; diisobutylaluminium hydride; sodium hydrogencarbonate; caesium carbonate; toluene-4-sulfonic acid; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; lithium diisopropyl amide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol;
DOI:10.1021/ja990789h