N-4-<<(benzyloxy)carbonyl>amino>phenylacetate N-hydroxysuccinimidyl ester

Base Information

Chemical Name:N-4-<<(benzyloxy)carbonyl>amino>phenylacetate N-hydroxysuccinimidyl ester
CAS No.:149414-91-5
Molecular Formula:C₂₀H₁₈N₂O₆
Molecular Weight:382.373
Hs Code.:

Synonyms:N-4-<<(benzyloxy)carbonyl>amino>phenylacetate N-hydroxysuccinimidyl ester

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Chemical Property of N-4-<<(benzyloxy)carbonyl>amino>phenylacetate N-hydroxysuccinimidyl ester

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Technology Process of N-4-<<(benzyloxy)carbonyl>amino>phenylacetate N-hydroxysuccinimidyl ester

There total 6 articles about N-4-<<(benzyloxy)carbonyl>amino>phenylacetate N-hydroxysuccinimidyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 6066-82-6
1-hydroxy-pyrrolidine-2,5-dione

: 17859-70-0
N-4-<<(benzyloxy)carbonyl>amino>phenylacetic acid

: 149414-91-5
N-4-<<(benzyloxy)carbonyl>amino>phenylacetate N-hydroxysuccinimidyl ester

Guidance literature:: With N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; In N,N-dimethyl-formamide; for 16h;
DOI:10.1021/jm980673g

Reference yield:

: 1197-55-3
4-aminophenylacetic acid

: 149414-91-5
N-4-<<(benzyloxy)carbonyl>amino>phenylacetate N-hydroxysuccinimidyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / NaOH / H₂O; dioxane / 2 h / ice bath

2: DCC / tetrahydrofuran / 2 h / 20 °C

With sodium hydroxide; dicyclohexyl-carbodiimide; In tetrahydrofuran; 1,4-dioxane; water;
DOI:10.1021/ja011695m

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 149414-91-5
N-4-<<(benzyloxy)carbonyl>amino>phenylacetate N-hydroxysuccinimidyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / NaOH / H₂O; dioxane / 2 h / ice bath

2: DCC / tetrahydrofuran / 2 h / 20 °C

With sodium hydroxide; dicyclohexyl-carbodiimide; In tetrahydrofuran; 1,4-dioxane; water;
DOI:10.1021/ja011695m