4,5,6,7-tetrachloro-2'-p-tolyl-3'-phenyl-spiro<1,3-benzodioxole-2,4'(3'H)-quinazoline>

Base Information

Chemical Name:4,5,6,7-tetrachloro-2'-p-tolyl-3'-phenyl-spiro<1,3-benzodioxole-2,4'(3'H)-quinazoline>
CAS No.:77796-31-7
Molecular Formula:C₂₇H₁₆Cl₄N₂O₂
Molecular Weight:542.248
Hs Code.:

Synonyms:4,5,6,7-tetrachloro-2'-p-tolyl-3'-phenyl-spiro<1,3-benzodioxole-2,4'(3'H)-quinazoline>

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Chemical Property of 4,5,6,7-tetrachloro-2'-p-tolyl-3'-phenyl-spiro<1,3-benzodioxole-2,4'(3'H)-quinazoline>

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4,5,6,7-tetrachloro-2'-p-tolyl-3'-phenyl-spiro<1,3-benzodioxole-2,4'(3'H)-quinazoline>

There total 4 articles about 4,5,6,7-tetrachloro-2'-p-tolyl-3'-phenyl-spiro<1,3-benzodioxole-2,4'(3'H)-quinazoline> which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 2435-53-2
o-tetrachloroquinone

: 53628-21-0
2-(p-Tolyl)-3-phenyl-3H,4H-quinazoline-4-thione

: 77796-31-7
4,5,6,7-tetrachloro-2'-p-tolyl-3'-phenyl-spiro<1,3-benzodioxole-2,4'(3'H)-quinazoline>

Guidance literature:: With dibenzoyl peroxide; In toluene; for 8h; Heating;

Reference yield:

: 2435-53-2
o-tetrachloroquinone

: 77796-31-7
4,5,6,7-tetrachloro-2'-p-tolyl-3'-phenyl-spiro<1,3-benzodioxole-2,4'(3'H)-quinazoline>

Guidance literature:: Multi-step reaction with 3 steps

1: 53 percent / benzoyl peroxide / toluene / 8 h / Heating

2: ethanol / 3 h / Heating

3: 48 percent / benzoyl peroxide / toluene / 8 h / Heating

With dibenzoyl peroxide; In ethanol; toluene;

Reference yield:

: 77796-32-8
4,5,6,7-tetrachloro-2'-p-anisyl-3'-phenyl-spiro<1,3-benzodioxole-2,4'(3'H)-quinazoline>

: 77796-31-7
4,5,6,7-tetrachloro-2'-p-tolyl-3'-phenyl-spiro<1,3-benzodioxole-2,4'(3'H)-quinazoline>

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol / 3 h / Heating

2: 48 percent / benzoyl peroxide / toluene / 8 h / Heating

With dibenzoyl peroxide; In ethanol; toluene;