1,1-dimethyl-2-[((indan-2-yl)(phenyl)amino)methyl]piperidinium iodide

Base Information

Chemical Name:1,1-dimethyl-2-[((indan-2-yl)(phenyl)amino)methyl]piperidinium iodide
CAS No.:1393836-33-3
Molecular Formula:C₂₃H₃₁N₂*I
Molecular Weight:462.417
Hs Code.:

Synonyms:1,1-dimethyl-2-[((indan-2-yl)(phenyl)amino)methyl]piperidinium iodide

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Chemical Property of 1,1-dimethyl-2-[((indan-2-yl)(phenyl)amino)methyl]piperidinium iodide

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Technology Process of 1,1-dimethyl-2-[((indan-2-yl)(phenyl)amino)methyl]piperidinium iodide

There total 9 articles about 1,1-dimethyl-2-[((indan-2-yl)(phenyl)amino)methyl]piperidinium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.62%

: 313257-47-5
N-[(1-methylpiperidin-2-yl)methyl]-N-phenylindan-2-yl-amine

: 74-88-4
methyl iodide

: 1393836-33-3
1,1-dimethyl-2-[((indan-2-yl)(phenyl)amino)methyl]piperidinium iodide

Guidance literature:: In 1,2-dichloro-ethane; at 20 ℃; for 16h;

Reference yield:

: 615-13-4
2-indanone

: 1393836-33-3
1,1-dimethyl-2-[((indan-2-yl)(phenyl)amino)methyl]piperidinium iodide

Guidance literature:: Multi-step reaction with 5 steps

1.1: acetic acid; sodium tris(acetoxy)borohydride / dichloromethane / 16 h / 20 °C / Cooling with ice

2.1: sodium amide / toluene / 3 h / 0 - 20 °C

2.2: 16 h / Reflux

3.1: ammonium formate / palladium 10% on activated carbon / methanol / 3 h / Reflux; Inert atmosphere

4.1: acetic acid; sodium tris(acetoxy)borohydride / water; 1,2-dichloro-ethane / 16 h / 20 °C

5.1: 1,2-dichloro-ethane / 16 h / 20 °C

With ammonium formate; sodium tris(acetoxy)borohydride; sodium amide; acetic acid; palladium 10% on activated carbon; In methanol; dichloromethane; water; 1,2-dichloro-ethane; toluene;

Reference yield:

: 62-53-3
aniline

: 1393836-33-3
1,1-dimethyl-2-[((indan-2-yl)(phenyl)amino)methyl]piperidinium iodide

Guidance literature:: Multi-step reaction with 5 steps

1.1: acetic acid; sodium tris(acetoxy)borohydride / dichloromethane / 16 h / 20 °C / Cooling with ice

2.1: sodium amide / toluene / 3 h / 0 - 20 °C

2.2: 16 h / Reflux

3.1: ammonium formate / palladium 10% on activated carbon / methanol / 3 h / Reflux; Inert atmosphere

4.1: acetic acid; sodium tris(acetoxy)borohydride / water; 1,2-dichloro-ethane / 16 h / 20 °C

5.1: 1,2-dichloro-ethane / 16 h / 20 °C

With ammonium formate; sodium tris(acetoxy)borohydride; sodium amide; acetic acid; palladium 10% on activated carbon; In methanol; dichloromethane; water; 1,2-dichloro-ethane; toluene;