N-{(1S,2E)-4-(benzyloxy)-1-[(1S,2E)-3-iodo-1-methylprop-2-en-1-yl]-2-methylbut-2-en-1-yl}-2-nitroaniline

Base Information

Chemical Name:N-{(1S,2E)-4-(benzyloxy)-1-[(1S,2E)-3-iodo-1-methylprop-2-en-1-yl]-2-methylbut-2-en-1-yl}-2-nitroaniline
CAS No.:1072091-35-0
Molecular Formula:C₂₂H₂₅IN₂O₅S
Molecular Weight:556.421
Hs Code.:

Synonyms:N-{(1S,2E)-4-(benzyloxy)-1-[(1S,2E)-3-iodo-1-methylprop-2-en-1-yl]-2-methylbut-2-en-1-yl}-2-nitroaniline

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Chemical Property of N-{(1S,2E)-4-(benzyloxy)-1-[(1S,2E)-3-iodo-1-methylprop-2-en-1-yl]-2-methylbut-2-en-1-yl}-2-nitroaniline

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Technology Process of N-{(1S,2E)-4-(benzyloxy)-1-[(1S,2E)-3-iodo-1-methylprop-2-en-1-yl]-2-methylbut-2-en-1-yl}-2-nitroaniline

There total 8 articles about N-{(1S,2E)-4-(benzyloxy)-1-[(1S,2E)-3-iodo-1-methylprop-2-en-1-yl]-2-methylbut-2-en-1-yl}-2-nitroaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1072091-18-9
C₁₆H₂₂INO

: 1694-92-4
2-Nitrobenzenesulfonyl chloride

: 1072091-35-0
N-{(1S,2E)-4-(benzyloxy)-1-[(1S,2E)-3-iodo-1-methylprop-2-en-1-yl]-2-methylbut-2-en-1-yl}-2-nitroaniline

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 3h;

Reference yield:

: 1072091-12-3
(2R,3S,4E)-6-(benzyloxy)-3-[(4-methoxyphenyl)amino]-2,4-dimethylhex-4-en-1-ol

: 1072091-35-0
N-{(1S,2E)-4-(benzyloxy)-1-[(1S,2E)-3-iodo-1-methylprop-2-en-1-yl]-2-methylbut-2-en-1-yl}-2-nitroaniline

Guidance literature:: Multi-step reaction with 5 steps

1.1: sulfuric acid; periodic acid / water; acetonitrile / 1.5 h / 20 °C

1.2: 8 h / 20 °C

2.1: Dess-Martin periodane / dichloromethane / 0.17 h / 20 °C

3.1: chromium dichloride / tetrahydrofuran / 5.5 h / 0 - 20 °C

4.1: hydrogenchloride / ethyl acetate / 1 h / 20 °C

5.1: triethylamine / dichloromethane / 3 h / 20 °C

With chromium dichloride; hydrogenchloride; sulfuric acid; Dess-Martin periodane; periodic acid; triethylamine; In tetrahydrofuran; dichloromethane; water; ethyl acetate; acetonitrile;

Reference yield:

: 1072091-09-8
N-[(1S,2E)-4-(benzyloxy)-1-((1R)-2-{[tert-butyl(dimethyl)silyl]oxy}-1-methylethyl)-2-methylbut-2-en-1-yl]-4-methoxyaniline

: 1072091-35-0
N-{(1S,2E)-4-(benzyloxy)-1-[(1S,2E)-3-iodo-1-methylprop-2-en-1-yl]-2-methylbut-2-en-1-yl}-2-nitroaniline

Guidance literature:: Multi-step reaction with 6 steps

1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C

2.1: sulfuric acid; periodic acid / water; acetonitrile / 1.5 h / 20 °C

2.2: 8 h / 20 °C

3.1: Dess-Martin periodane / dichloromethane / 0.17 h / 20 °C

4.1: chromium dichloride / tetrahydrofuran / 5.5 h / 0 - 20 °C

5.1: hydrogenchloride / ethyl acetate / 1 h / 20 °C

6.1: triethylamine / dichloromethane / 3 h / 20 °C

With chromium dichloride; hydrogenchloride; sulfuric acid; tetrabutyl ammonium fluoride; Dess-Martin periodane; periodic acid; triethylamine; In tetrahydrofuran; dichloromethane; water; ethyl acetate; acetonitrile;