Thiobenzoic acid S-(4-{(2R,4S,5R)-5-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-4-hydroxy-tetrahydro-furan-2-yl}-phenyl) ester

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Chemical Name:Thiobenzoic acid S-(4-{(2R,4S,5R)-5-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-4-hydroxy-tetrahydro-furan-2-yl}-phenyl) ester
CAS No.:705971-59-1
Molecular Formula:C₃₉H₃₆O₆S
Molecular Weight:632.777
Hs Code.:

Synonyms:Thiobenzoic acid S-(4-{(2R,4S,5R)-5-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-4-hydroxy-tetrahydro-furan-2-yl}-phenyl) ester

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Chemical Property of Thiobenzoic acid S-(4-{(2R,4S,5R)-5-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-4-hydroxy-tetrahydro-furan-2-yl}-phenyl) ester

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Technology Process of Thiobenzoic acid S-(4-{(2R,4S,5R)-5-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-4-hydroxy-tetrahydro-furan-2-yl}-phenyl) ester

There total 7 articles about Thiobenzoic acid S-(4-{(2R,4S,5R)-5-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-4-hydroxy-tetrahydro-furan-2-yl}-phenyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 705971-58-0
Thiobenzoic acid S-[4-((2R,4S,5R)-4-hydroxy-5-hydroxymethyl-tetrahydro-furan-2-yl)-phenyl] ester

: 705971-59-1
Thiobenzoic acid S-(4-{(2R,4S,5R)-5-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-4-hydroxy-tetrahydro-furan-2-yl}-phenyl) ester

Guidance literature:: With pyridine; at 20 ℃; for 1h;
DOI:10.1016/j.tet.2004.12.038

Reference yield:

: 4330-34-1
methyl 3,5-di-O-toluoyl-2-deoxy-D-ribofuranose

: 705971-59-1
Thiobenzoic acid S-(4-{(2R,4S,5R)-5-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-4-hydroxy-tetrahydro-furan-2-yl}-phenyl) ester

Guidance literature:: Multi-step reaction with 4 steps

1: 18 percent / tin(IV) chloride / CH₂Cl₂ / 8 h / -15 °C

2: 37 percent / LiAlH₄ / tetrahydrofuran / 1 h / 4 °C

3: 71 percent / diisopropylethylamine / tetrahydrofuran / 1 h / 20 °C

4: 96 percent / pyridine / 1 h / 20 °C

With pyridine; lithium aluminium tetrahydride; tin(IV) chloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; 1: Friedel-Crafts alkylation;
DOI:10.1016/j.tet.2004.12.038

Reference yield:

: 882-33-7
diphenyldisulfane

: 705971-59-1
Thiobenzoic acid S-(4-{(2R,4S,5R)-5-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-4-hydroxy-tetrahydro-furan-2-yl}-phenyl) ester

Guidance literature:: Multi-step reaction with 4 steps

1: 18 percent / tin(IV) chloride / CH₂Cl₂ / 8 h / -15 °C

2: 37 percent / LiAlH₄ / tetrahydrofuran / 1 h / 4 °C

3: 71 percent / diisopropylethylamine / tetrahydrofuran / 1 h / 20 °C

4: 96 percent / pyridine / 1 h / 20 °C

With pyridine; lithium aluminium tetrahydride; tin(IV) chloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; 1: Friedel-Crafts alkylation;
DOI:10.1016/j.tet.2004.12.038