cyclohexyl 2-(2-acetoxyacetamido)-2-deoxy-1-thio-α-D-glucopyranoside

Base Information

• Chemical Name: cyclohexyl 2-(2-acetoxyacetamido)-2-deoxy-1-thio-α-D-glucopyranoside
• CAS No.: 862269-21-4
• Molecular Formula: C₁₆H₂₇NO₇S
• Molecular Weight: 377.459
• Mol file: 862269-21-4.mol

Synonyms:cyclohexyl 2-(2-acetoxyacetamido)-2-deoxy-1-thio-α-D-glucopyranoside

Chemical Property of cyclohexyl 2-(2-acetoxyacetamido)-2-deoxy-1-thio-α-D-glucopyranoside

Chemical Property:

Purity/Quality:

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Technology Process of cyclohexyl 2-(2-acetoxyacetamido)-2-deoxy-1-thio-α-D-glucopyranoside

There total 1 articles about cyclohexyl 2-(2-acetoxyacetamido)-2-deoxy-1-thio-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

acetoxyacetic acid (13831-30-6) + cyclohexyl 2-amino-2-deoxy-1-thio-α-D-glucopyranoside (479255-66-8) → cyclohexyl 2-(2-acetoxyacetamido)-2-deoxy-1-thio-α-D-glucopyranoside (862269-21-4)

Guidance literature:

With N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In N,N-dimethyl-formamide; at 0 - 23 ℃; for 3h;

DOI:10.1081/CAR-200059965

Reference yield: 92.0%

cyclohexyl 2-(2-acetoxyacetamido)-2-deoxy-1-thio-α-D-glucopyranoside (862269-21-4) → cyclohexyl 2-deoxy-2-(2-hydroxyacetamido)-1-thio-α-D-glucopyranoside

Guidance literature:

With sodium methylate; In methanol; at 0 - 23 ℃;

DOI:10.1081/CAR-200059965

Reference yield: 55.0%

cyclohexyl 2-(2-acetoxyacetamido)-2-deoxy-1-thio-α-D-glucopyranoside (862269-21-4) → cyclohexyl 2-deoxy-2-(2-hydroxyethylamino)-1-thio-α-D-glucopyranoside

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; for 48h; Heating;

DOI:10.1081/CAR-200059965

upstream raw materials:

acetoxyacetic acid

cyclohexyl 2-amino-2-deoxy-1-thio-α-D-glucopyranoside