Technology Process of Zn(N4C20H8(C6H3(C(CH3)3)2)3C6H4N3C2HC6H4CHO)
There total 8 articles about Zn(N4C20H8(C6H3(C(CH3)3)2)3C6H4N3C2HC6H4CHO) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
copper(l) iodide; sodium L-ascorbate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine;
In
water; dimethyl sulfoxide;
at 80 ℃;
for 2h;
Microwave irradiation;
Sonication;
Inert atmosphere;
DOI:10.1021/ja202485s
- Guidance literature:
-
Multi-step reaction with 2 steps
1: zinc(II) acetate dihydrate / methanol / 1 h / Reflux
2: copper(l) iodide; sodium L-ascorbate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine / water; dimethyl sulfoxide / 2 h / 80 °C / Microwave irradiation; Sonication; Inert atmosphere
With
copper(l) iodide; zinc(II) acetate dihydrate; sodium L-ascorbate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine;
In
methanol; water; dimethyl sulfoxide;
2: Huisgen cycloaddition;
DOI:10.1021/ja202485s
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: trifluoroacetic acid / dichloromethane / 1.5 h / 20 °C / Inert atmosphere
2.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 1 h / 20 °C
3.1: hydrogenchloride; water / ethanol / 17 h / Reflux
4.1: trifluoroacetic acid; sodium nitrite / water / 0.25 h / 0 °C
4.2: 1 h / 0 °C
5.1: zinc(II) acetate dihydrate / methanol / 1 h / Reflux
6.1: copper(l) iodide; sodium L-ascorbate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine / water; dimethyl sulfoxide / 2 h / 80 °C / Microwave irradiation; Sonication; Inert atmosphere
With
hydrogenchloride; copper(l) iodide; water; zinc(II) acetate dihydrate; sodium L-ascorbate; trifluoroacetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium nitrite; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine;
In
methanol; ethanol; dichloromethane; water; dimethyl sulfoxide;
6.1: Huisgen cycloaddition;
DOI:10.1021/ja202485s
