2-((1S,2R,4R)-2-Hydroxy-7,7-dimethyl-bicyclo[2.2.1]hept-1-ylmethanesulfonyl)-1-phenyl-ethanone

Base Information

Chemical Name:2-((1S,2R,4R)-2-Hydroxy-7,7-dimethyl-bicyclo[2.2.1]hept-1-ylmethanesulfonyl)-1-phenyl-ethanone
CAS No.:129840-07-9
Molecular Formula:C₁₈H₂₄O₄S
Molecular Weight:336.452
Hs Code.:

Synonyms:2-((1S,2R,4R)-2-Hydroxy-7,7-dimethyl-bicyclo[2.2.1]hept-1-ylmethanesulfonyl)-1-phenyl-ethanone

Suppliers and Price of 2-((1S,2R,4R)-2-Hydroxy-7,7-dimethyl-bicyclo[2.2.1]hept-1-ylmethanesulfonyl)-1-phenyl-ethanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-((1S,2R,4R)-2-Hydroxy-7,7-dimethyl-bicyclo[2.2.1]hept-1-ylmethanesulfonyl)-1-phenyl-ethanone

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-((1S,2R,4R)-2-Hydroxy-7,7-dimethyl-bicyclo[2.2.1]hept-1-ylmethanesulfonyl)-1-phenyl-ethanone

There total 3 articles about 2-((1S,2R,4R)-2-Hydroxy-7,7-dimethyl-bicyclo[2.2.1]hept-1-ylmethanesulfonyl)-1-phenyl-ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 129839-99-2
(-)-10-(Phenacylthio)isoborneol

: 129840-07-9
2-((1S,2R,4R)-2-Hydroxy-7,7-dimethyl-bicyclo[2.2.1]hept-1-ylmethanesulfonyl)-1-phenyl-ethanone

: 129840-00-2,129840-01-3
2-((R)-(1R,2S,4S)-2-Hydroxy-7,7-dimethyl-bicyclo[2.2.1]hept-1-ylmethanesulfinyl)-1-phenyl-ethanone

: 129840-00-2,129840-01-3
2-((S)-(1R,2S,4S)-2-Hydroxy-7,7-dimethyl-bicyclo[2.2.1]hept-1-ylmethanesulfinyl)-1-phenyl-ethanone

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at -70 - -10 ℃; for 2h;
DOI:10.1055/s-1990-26864

Reference yield:

: 71242-58-5
(1S,2R,4R)-(-)-10-mercaptoisoboneol

: 129840-07-9
2-((1S,2R,4R)-2-Hydroxy-7,7-dimethyl-bicyclo[2.2.1]hept-1-ylmethanesulfonyl)-1-phenyl-ethanone

Guidance literature:: Multi-step reaction with 2 steps

1: 1) NaH / 1) benzene,DMF, 0 deg C, 20 min,2) r.t., 3h

2: 3-chloroperoxybenzoic acid / CH₂Cl₂ / 2 h / -70 - -10 °C

With sodium hydride; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1055/s-1990-26864

Reference yield:

: 70-11-1
α-bromoacetophenone

: 129840-07-9
2-((1S,2R,4R)-2-Hydroxy-7,7-dimethyl-bicyclo[2.2.1]hept-1-ylmethanesulfonyl)-1-phenyl-ethanone

Guidance literature:: Multi-step reaction with 2 steps

1: 1) NaH / 1) benzene,DMF, 0 deg C, 20 min,2) r.t., 3h

2: 3-chloroperoxybenzoic acid / CH₂Cl₂ / 2 h / -70 - -10 °C

With sodium hydride; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1055/s-1990-26864