1-⁽¹³⁾C-1-(4'-amino-3',5'-dichlorophenyl)-2-(tert-butylamino)ethanone hydrochloride

Base Information

• Chemical Name: 1-⁽¹³⁾C-1-(4'-amino-3',5'-dichlorophenyl)-2-(tert-butylamino)ethanone hydrochloride
• CAS No.: 1319718-89-2
• Molecular Formula: C₁₂H₁₆Cl₂N₂O*ClH
• Molecular Weight: 312.628

Synonyms:1-⁽¹³⁾C-1-(4'-amino-3',5'-dichlorophenyl)-2-(tert-butylamino)ethanone hydrochloride

Chemical Property of 1-⁽¹³⁾C-1-(4'-amino-3',5'-dichlorophenyl)-2-(tert-butylamino)ethanone hydrochloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-⁽¹³⁾C-1-(4'-amino-3',5'-dichlorophenyl)-2-(tert-butylamino)ethanone hydrochloride

There total 5 articles about 1-⁽¹³⁾C-1-(4'-amino-3',5'-dichlorophenyl)-2-(tert-butylamino)ethanone hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(13)C-4'-amino-2-bromo-3',5'-dichloroacetophenone (1319718-87-0) + tert-butylamine (75-64-9) → 1-(13)C-1-(4'-amino-3',5'-dichlorophenyl)-2-(tert-butylamino)ethanone hydrochloride (1319718-89-2)

Guidance literature:

1-⁽¹³⁾C-4'-amino-2-bromo-3',5'-dichloroacetophenone; tert-butylamine; In chloroform; at 50 ℃; for 24h;

With hydrogenchloride; In diethyl ether; chloroform;

DOI:10.1016/j.tet.2011.05.118

Reference yield:

4'-aminoacetophen[13C-carbonyl]one (861435-57-6) → 1-(13)C-1-(4'-amino-3',5'-dichlorophenyl)-2-(tert-butylamino)ethanone hydrochloride (1319718-89-2)

Guidance literature:

Multi-step reaction with 3 steps

1: hydrogenchloride; N-chloro-succinimide / water / 10 h / 50 °C

2: bromine / dichloromethane / 20 °C

3: chloroform / 24 h / 50 °C

With hydrogenchloride; N-chloro-succinimide; bromine; In dichloromethane; chloroform; water;

DOI:10.1016/j.tet.2011.05.118

Reference yield:

1-(13)C-4'-acetamidoacetophenone (1319718-85-8) → 1-(13)C-1-(4'-amino-3',5'-dichlorophenyl)-2-(tert-butylamino)ethanone hydrochloride (1319718-89-2)

Guidance literature:

Multi-step reaction with 4 steps

1: sodium hydroxide / methanol / 20 h / 50 °C

2: hydrogenchloride; N-chloro-succinimide / water / 10 h / 50 °C

3: bromine / dichloromethane / 20 °C

4: chloroform / 24 h / 50 °C

With hydrogenchloride; N-chloro-succinimide; bromine; sodium hydroxide; In methanol; dichloromethane; chloroform; water;

DOI:10.1016/j.tet.2011.05.118

upstream raw materials:

4'-aminoacetophen[13C-carbonyl]one

1-⁽¹³⁾C-4'-amino-2-bromo-3',5'-dichloroacetophenone

tert-butylamine

1-⁽¹³⁾C-4'-acetamidoacetophenone

Downstream raw materials:

1-⁽¹³⁾C-1-(4'-amino-3',5'-dichlorophenyl)-2-(tert-butylamine)ethanol hydrochloride

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 1319718-89-2 1-⁽¹³⁾C-1-(4'-amino-3',5'-dichlorophenyl)-2-(tert-butylamino)ethanone hydrochloride

Send

Send

Metric Ton KG G Pound L ML

Send

Send