N-[3-(2-amino-4-bromo-phenylamino)-5-(5-methyl-furan-2-yl)-phenyl]-acetamide

Base Information

Chemical Name:N-[3-(2-amino-4-bromo-phenylamino)-5-(5-methyl-furan-2-yl)-phenyl]-acetamide
CAS No.:1430727-85-7
Molecular Formula:C₁₉H₁₈BrN₃O₂
Molecular Weight:400.275
Hs Code.:

Synonyms:N-[3-(2-amino-4-bromo-phenylamino)-5-(5-methyl-furan-2-yl)-phenyl]-acetamide

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Chemical Property of N-[3-(2-amino-4-bromo-phenylamino)-5-(5-methyl-furan-2-yl)-phenyl]-acetamide

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Technology Process of N-[3-(2-amino-4-bromo-phenylamino)-5-(5-methyl-furan-2-yl)-phenyl]-acetamide

There total 7 articles about N-[3-(2-amino-4-bromo-phenylamino)-5-(5-methyl-furan-2-yl)-phenyl]-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1430727-84-6
N-[3-(4-bromo-2-nitro-phenylamino)-5-(5-methyl-furan-2-yl)-phenyl]-acetamide

: 1430727-85-7
N-[3-(2-amino-4-bromo-phenylamino)-5-(5-methyl-furan-2-yl)-phenyl]-acetamide

Guidance literature:: With iron; calcium chloride; In ethanol; water; at 80 ℃; for 2h;

Reference yield:

: 18242-39-2
3,5-dinitrobromobenzene

: 1430727-85-7
N-[3-(2-amino-4-bromo-phenylamino)-5-(5-methyl-furan-2-yl)-phenyl]-acetamide

Guidance literature:: Multi-step reaction with 6 steps

1: acetic acid; iron / acetic acid / 0.5 h / 90 °C

2: 0.5 h / 0 - 20 °C

3: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / water; 1,2-dimethoxyethane; ethyl acetate / 2 h / 100 °C / Inert atmosphere

4: hydrogenchloride; palladium 10% on activated carbon / methanol / 6 h / 20 °C

5: potassium fluoride / N,N-dimethyl-formamide / 100 °C

6: water; calcium chloride; iron / ethanol / 2 h / 80 °C

With hydrogenchloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium fluoride; palladium 10% on activated carbon; water; iron; sodium carbonate; acetic acid; calcium chloride; In methanol; 1,2-dimethoxyethane; ethanol; water; acetic acid; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 99-65-0
meta-dinitrobenzene

: 1430727-85-7
N-[3-(2-amino-4-bromo-phenylamino)-5-(5-methyl-furan-2-yl)-phenyl]-acetamide

Guidance literature:: Multi-step reaction with 7 steps

1: sulfuric acid; 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione / 12.5 h / 0 - 20 °C

2: acetic acid; iron / acetic acid / 0.5 h / 90 °C

3: 0.5 h / 0 - 20 °C

4: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / water; 1,2-dimethoxyethane; ethyl acetate / 2 h / 100 °C / Inert atmosphere

5: hydrogenchloride; palladium 10% on activated carbon / methanol / 6 h / 20 °C

6: potassium fluoride / N,N-dimethyl-formamide / 100 °C

7: water; calcium chloride; iron / ethanol / 2 h / 80 °C

With hydrogenchloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium fluoride; 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; sulfuric acid; palladium 10% on activated carbon; water; iron; sodium carbonate; acetic acid; calcium chloride; In methanol; 1,2-dimethoxyethane; ethanol; water; acetic acid; ethyl acetate; N,N-dimethyl-formamide;