Technology Process of C23H20N8O2
There total 4 articles about C23H20N8O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium azide; ammonium chloride; lithium chloride;
In
N,N-dimethyl-formamide;
at 100 ℃;
for 18h;
Inert atmosphere;
DOI:10.1016/j.bmc.2012.11.054
- Guidance literature:
-
Multi-step reaction with 3 steps
1: caesium carbonate / N,N-dimethyl-formamide / 9.5 h / 0 - 80 °C
2: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate / N,N-dimethyl-formamide / 80 °C / Inert atmosphere
3: ammonium chloride; lithium chloride; sodium azide / N,N-dimethyl-formamide / 18 h / 100 °C / Inert atmosphere
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate; sodium azide; ammonium chloride; caesium carbonate; lithium chloride;
In
N,N-dimethyl-formamide;
2: |Suzuki Coupling;
DOI:10.1016/j.bmc.2012.11.054
- Guidance literature:
-
Multi-step reaction with 2 steps
1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate / N,N-dimethyl-formamide / 80 °C / Inert atmosphere
2: ammonium chloride; lithium chloride; sodium azide / N,N-dimethyl-formamide / 18 h / 100 °C / Inert atmosphere
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate; sodium azide; ammonium chloride; lithium chloride;
In
N,N-dimethyl-formamide;
1: |Suzuki Coupling;
DOI:10.1016/j.bmc.2012.11.054
