tetracarbonyl-μ,μ'-(1,3-di(2,4,6-tri-t-butylphenyl)-1,3-diphosphaallyl)dinickel

Base Information

Chemical Name:tetracarbonyl-μ,μ'-(1,3-di(2,4,6-tri-t-butylphenyl)-1,3-diphosphaallyl)dinickel
CAS No.:112285-05-9
Molecular Formula:C₇₈H₁₁₈Ni₂O₄P₄
Molecular Weight:1361.07
Hs Code.:

Synonyms:tetracarbonyl-μ,μ'-(1,3-di(2,4,6-tri-t-butylphenyl)-1,3-diphosphaallyl)dinickel

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Chemical Property of tetracarbonyl-μ,μ'-(1,3-di(2,4,6-tri-t-butylphenyl)-1,3-diphosphaallyl)dinickel

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Technology Process of tetracarbonyl-μ,μ'-(1,3-di(2,4,6-tri-t-butylphenyl)-1,3-diphosphaallyl)dinickel

There total 1 articles about tetracarbonyl-μ,μ'-(1,3-di(2,4,6-tri-t-butylphenyl)-1,3-diphosphaallyl)dinickel which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

: 96164-77-1,93554-05-3
1,3-di(2,4,6-tri-t-butylphenyl)-3-chloro-1,3-diphosphapropene

: 13463-39-3,71564-36-8
tetracarbonyl nickel

: 112285-05-9
tetracarbonyl-μ,μ'-(1,3-di(2,4,6-tri-t-butylphenyl)-1,3-diphosphaallyl)dinickel

Guidance literature:: In 1,2-dichloro-ethane; byproducts: CO, NiCl2; under inert gas, to soln. of (t-Bu)3C6H2PCHP(Cl)C6H2(t-Bu)3 in ClCH2CH2Cl Ni(CO)4 added with stirring, heated at 65°C for 24 h, cooled; filtered, concd. with heating, after standing for many days crystals sepd., washed repeatedly with n-hexane, dried; elem. anal.;
DOI:10.1016/S0022-328X(00)99607-4