C₃₃H₅₄O₈S₂Si

Base Information

Chemical Name:C₃₃H₅₄O₈S₂Si
CAS No.:1392829-19-4
Molecular Formula:C₃₃H₅₄O₈S₂Si
Molecular Weight:671.004
Hs Code.:

C<sub>33</sub>H<sub>54</sub>O<sub>8</sub>S<sub>2</sub>Si

Synonyms:C₃₃H₅₄O₈S₂Si

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Chemical Property of C₃₃H₅₄O₈S₂Si

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Technology Process of C₃₃H₅₄O₈S₂Si

There total 16 articles about C₃₃H₅₄O₈S₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1392829-10-5
C₃₃H₅₆O₈S₂Si

: 1392829-19-4
C₃₃H₅₄O₈S₂Si

Guidance literature:: With pyridine; Dess-Martin periodane; In dichloromethane; at 0 - 20 ℃;
DOI:10.1016/j.tetlet.2012.06.005

Reference yield:

: C₂₀H₃₀O₅Si

: 1392829-19-4
C₃₃H₅₄O₈S₂Si

Guidance literature:: Multi-step reaction with 10 steps

1.1: boron trifluoride diethyl etherate / diethyl ether / 0 °C

2.1: sodium periodate; ruthenium trichloride; water; zinc(II) chloride / ethyl acetate; acetonitrile / 0 °C

3.1: toluene-4-sulfonic acid / tetrahydrofuran / 40 °C

4.1: sodium tetrahydroborate / methanol; dichloromethane / 0 °C

5.1: sodium hydride / tetrahydrofuran / 0 °C

5.2: 0 - 20 °C

6.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / benzene / 80 °C

7.1: LiDBB / tetrahydrofuran / -78 °C

8.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / dichloromethane / 0 - 20 °C

9.1: n-butyllithium / tetrahydrofuran / 20 °C

9.2: -78 - 0 °C

10.1: pyridine; Dess-Martin periodane / dichloromethane / 0 - 20 °C

With pyridine; ruthenium trichloride; sodium tetrahydroborate; sodium periodate; n-butyllithium; 2,2'-azobis(isobutyronitrile); boron trifluoride diethyl etherate; water; tri-n-butyl-tin hydride; sulfur trioxide pyridine complex; sodium hydride; Dess-Martin periodane; toluene-4-sulfonic acid; dimethyl sulfoxide; triethylamine; zinc(II) chloride; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; ethyl acetate; acetonitrile; benzene; 6.1: Barton-McCombie deoxygenation / 8.1: Parikh-Doering oxidation;
DOI:10.1016/j.tetlet.2012.06.005

Reference yield:

: 1392829-16-1
C₂₄H₃₈O₇Si

: 1392829-19-4
C₃₃H₅₄O₈S₂Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium tetrahydroborate / methanol; dichloromethane / 0 °C

2.1: sodium hydride / tetrahydrofuran / 0 °C

2.2: 0 - 20 °C

3.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / benzene / 80 °C

4.1: LiDBB / tetrahydrofuran / -78 °C

5.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / dichloromethane / 0 - 20 °C

6.1: n-butyllithium / tetrahydrofuran / 20 °C

6.2: -78 - 0 °C

7.1: pyridine; Dess-Martin periodane / dichloromethane / 0 - 20 °C

With pyridine; sodium tetrahydroborate; n-butyllithium; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; sulfur trioxide pyridine complex; sodium hydride; Dess-Martin periodane; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; methanol; dichloromethane; benzene; 3.1: Barton-McCombie deoxygenation / 5.1: Parikh-Doering oxidation;
DOI:10.1016/j.tetlet.2012.06.005