cis-1-<1-<<(p-nitrobenzyl)oxy>carbonyl>-2-mesylpropenyl>-3-phenoxyacetamido-4-styryl-2-azetidinone

Base Information

Chemical Name:cis-1-<1-<<(p-nitrobenzyl)oxy>carbonyl>-2-mesylpropenyl>-3-phenoxyacetamido-4-styryl-2-azetidinone
CAS No.:82730-18-5
Molecular Formula:C₃₁H₂₉N₃O₁₀S
Molecular Weight:635.651
Hs Code.:

Synonyms:cis-1-<1-<<(p-nitrobenzyl)oxy>carbonyl>-2-mesylpropenyl>-3-phenoxyacetamido-4-styryl-2-azetidinone

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Chemical Property of cis-1-<1-<<(p-nitrobenzyl)oxy>carbonyl>-2-mesylpropenyl>-3-phenoxyacetamido-4-styryl-2-azetidinone

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Technology Process of cis-1-<1-<<(p-nitrobenzyl)oxy>carbonyl>-2-mesylpropenyl>-3-phenoxyacetamido-4-styryl-2-azetidinone

There total 7 articles about cis-1-<1-<<(p-nitrobenzyl)oxy>carbonyl>-2-mesylpropenyl>-3-phenoxyacetamido-4-styryl-2-azetidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.5%

: 82730-17-4
cis-1-<1-<<(p-nitrobenzyl)oxy>carbonyl>-2-hydroxypropenyl>-3-phenoxyacetamido-4-styryl-2-azetidinone

: 124-63-0
methanesulfonyl chloride

: 82730-18-5
cis-1-<1-<<(p-nitrobenzyl)oxy>carbonyl>-2-mesylpropenyl>-3-phenoxyacetamido-4-styryl-2-azetidinone

Guidance literature:: With dmap; In dichloromethane; for 0.0833333h;
DOI:10.1021/jo00142a015

Reference yield:

: 78905-32-5,79056-43-2,82730-11-8,82730-12-9
(2S,3S)-2-[(3S,4R)-3-Amino-2-oxo-4-((E)-styryl)-azetidin-1-yl]-3-hydroxy-butyric acid 4-nitro-benzyl ester

: 82730-18-5
cis-1-<1-<<(p-nitrobenzyl)oxy>carbonyl>-2-mesylpropenyl>-3-phenoxyacetamido-4-styryl-2-azetidinone

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / CH₂Cl₂ / 3 h / Ambient temperature

2: 44 percent / Jones reagent / acetone / 2 h

3: 74.5 percent / N,N-dimethylaminopyridine (DMAP) / CH₂Cl₂ / 0.08 h

With dmap; jones reagent; triethylamine; In dichloromethane; acetone;
DOI:10.1021/jo00142a015

Reference yield:

: 78905-33-6,79056-42-1,82730-13-0,82730-14-1
cis-1-<1-<<(p-nitrobenzyl)oxy>carbonyl>-2-hydroxypropyl>-3-(phenoxyacetamido)-4-styrylazetidin-2-one

: 82730-18-5
cis-1-<1-<<(p-nitrobenzyl)oxy>carbonyl>-2-mesylpropenyl>-3-phenoxyacetamido-4-styryl-2-azetidinone

Guidance literature:: Multi-step reaction with 2 steps

1: 44 percent / Jones reagent / acetone / 2 h

2: 74.5 percent / N,N-dimethylaminopyridine (DMAP) / CH₂Cl₂ / 0.08 h

With dmap; jones reagent; In dichloromethane; acetone;
DOI:10.1021/jo00142a015