tetramethyl 9,10-diphenyl-1,4;9,10-diepoxy-1,2,3,4,4a,9,9a,10-octahydroanthracene-2,3,6,7-tetracarboxylate

Base Information

Chemical Name:tetramethyl 9,10-diphenyl-1,4;9,10-diepoxy-1,2,3,4,4a,9,9a,10-octahydroanthracene-2,3,6,7-tetracarboxylate
CAS No.:83687-11-0
Molecular Formula:C₃₄H₃₀O₁₀
Molecular Weight:598.606
Hs Code.:

Synonyms:tetramethyl 9,10-diphenyl-1,4;9,10-diepoxy-1,2,3,4,4a,9,9a,10-octahydroanthracene-2,3,6,7-tetracarboxylate

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Chemical Property of tetramethyl 9,10-diphenyl-1,4;9,10-diepoxy-1,2,3,4,4a,9,9a,10-octahydroanthracene-2,3,6,7-tetracarboxylate

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Technology Process of tetramethyl 9,10-diphenyl-1,4;9,10-diepoxy-1,2,3,4,4a,9,9a,10-octahydroanthracene-2,3,6,7-tetracarboxylate

There total 5 articles about tetramethyl 9,10-diphenyl-1,4;9,10-diepoxy-1,2,3,4,4a,9,9a,10-octahydroanthracene-2,3,6,7-tetracarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1984-43-6,6828-11-1,51372-64-6,59275-03-5
dimethyl 7-oxabicyclo[2.2.1]hept-5-ene exo,exo-2,3-dicarboxylate

: 83687-09-6
dimethyl 1,3-diphenylisobenzofuran-5,6-dicarboxylate

: 83687-11-0
tetramethyl 9,10-diphenyl-1,4;9,10-diepoxy-1,2,3,4,4a,9,9a,10-octahydroanthracene-2,3,6,7-tetracarboxylate

Guidance literature:: In chloroform; for 48h; Heating;
DOI:10.1016/0040-4020(82)80224-X

Reference yield:

: 83687-05-2
4,5-dibenzoylphthalic acid

: 83687-11-0
tetramethyl 9,10-diphenyl-1,4;9,10-diepoxy-1,2,3,4,4a,9,9a,10-octahydroanthracene-2,3,6,7-tetracarboxylate

Guidance literature:: Multi-step reaction with 3 steps

2: 1.) KBH₄, 2.) H₂SO₄, 3.) CH₃ONa / 1.) CH₃OH, reflux,1 min.; 2.) CH₃OH, reflux,10 min.

3: 90 percent / CHCl₃ / 48 h / Heating

With potassium borohydride; sulfuric acid; sodium methylate; In chloroform;
DOI:10.1016/0040-4020(82)80224-X

Reference yield:

: 83687-07-4
dimethyl 4,5-dibenzoylphthalate

: 83687-11-0
tetramethyl 9,10-diphenyl-1,4;9,10-diepoxy-1,2,3,4,4a,9,9a,10-octahydroanthracene-2,3,6,7-tetracarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) KBH₄, 2.) H₂SO₄, 3.) CH₃ONa / 1.) CH₃OH, reflux,1 min.; 2.) CH₃OH, reflux,10 min.

2: 90 percent / CHCl₃ / 48 h / Heating

With potassium borohydride; sulfuric acid; sodium methylate; In chloroform;
DOI:10.1016/0040-4020(82)80224-X