tetramethyl 9,10-diphenyl-1,4-epoxy-1,2,3,4-tetrahydroanthracene-2,3,6,7-tetracarboxylate

Base Information

Chemical Name:tetramethyl 9,10-diphenyl-1,4-epoxy-1,2,3,4-tetrahydroanthracene-2,3,6,7-tetracarboxylate
CAS No.:83687-13-2
Molecular Formula:C₃₄H₂₈O₉
Molecular Weight:580.591
Hs Code.:

Synonyms:tetramethyl 9,10-diphenyl-1,4-epoxy-1,2,3,4-tetrahydroanthracene-2,3,6,7-tetracarboxylate

Suppliers and Price of tetramethyl 9,10-diphenyl-1,4-epoxy-1,2,3,4-tetrahydroanthracene-2,3,6,7-tetracarboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of tetramethyl 9,10-diphenyl-1,4-epoxy-1,2,3,4-tetrahydroanthracene-2,3,6,7-tetracarboxylate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of tetramethyl 9,10-diphenyl-1,4-epoxy-1,2,3,4-tetrahydroanthracene-2,3,6,7-tetracarboxylate

There total 8 articles about tetramethyl 9,10-diphenyl-1,4-epoxy-1,2,3,4-tetrahydroanthracene-2,3,6,7-tetracarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 83687-11-0
tetramethyl 9,10-diphenyl-1,4;9,10-diepoxy-1,2,3,4,4a,9,9a,10-octahydroanthracene-2,3,6,7-tetracarboxylate

: 83687-13-2
tetramethyl 9,10-diphenyl-1,4-epoxy-1,2,3,4-tetrahydroanthracene-2,3,6,7-tetracarboxylate

Guidance literature:: With phosphorus pentoxide; In dichloromethane; for 5h; Ambient temperature;
DOI:10.1016/0040-4020(82)80224-X

Reference yield:

: 83687-05-2
4,5-dibenzoylphthalic acid

: 83687-13-2
tetramethyl 9,10-diphenyl-1,4-epoxy-1,2,3,4-tetrahydroanthracene-2,3,6,7-tetracarboxylate

Guidance literature:: Multi-step reaction with 4 steps

2: 1.) KBH₄, 2.) H₂SO₄, 3.) CH₃ONa / 1.) CH₃OH, reflux,1 min.; 2.) CH₃OH, reflux,10 min.

3: 90 percent / CHCl₃ / 48 h / Heating

4: 1.) HBr / 1.) acetic acid, reflux 1 h; 2.) diethylether

With potassium borohydride; sulfuric acid; hydrogen bromide; sodium methylate; In chloroform;
DOI:10.1016/0040-4020(82)80224-X

Reference yield:

: 83687-07-4
dimethyl 4,5-dibenzoylphthalate

: 83687-13-2
tetramethyl 9,10-diphenyl-1,4-epoxy-1,2,3,4-tetrahydroanthracene-2,3,6,7-tetracarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) KBH₄, 2.) H₂SO₄, 3.) CH₃ONa / 1.) CH₃OH, reflux,1 min.; 2.) CH₃OH, reflux,10 min.

2: 90 percent / CHCl₃ / 48 h / Heating

3: 1.) HBr / 1.) acetic acid, reflux 1 h; 2.) diethylether

With potassium borohydride; sulfuric acid; hydrogen bromide; sodium methylate; In chloroform;
DOI:10.1016/0040-4020(82)80224-X