1-(2-deoxy-3,5-di-O-tetraisopropyldisiloxanyl-β-D-ribofuranosyl)-2-diphenylcarbamoyloxyimidazole

Base Information

Chemical Name:1-(2-deoxy-3,5-di-O-tetraisopropyldisiloxanyl-β-D-ribofuranosyl)-2-diphenylcarbamoyloxyimidazole
CAS No.:793674-24-5
Molecular Formula:C₃₃H₄₇N₃O₆Si₂
Molecular Weight:637.924
Hs Code.:

Synonyms:1-(2-deoxy-3,5-di-O-tetraisopropyldisiloxanyl-β-D-ribofuranosyl)-2-diphenylcarbamoyloxyimidazole

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Chemical Property of 1-(2-deoxy-3,5-di-O-tetraisopropyldisiloxanyl-β-D-ribofuranosyl)-2-diphenylcarbamoyloxyimidazole

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Technology Process of 1-(2-deoxy-3,5-di-O-tetraisopropyldisiloxanyl-β-D-ribofuranosyl)-2-diphenylcarbamoyloxyimidazole

There total 2 articles about 1-(2-deoxy-3,5-di-O-tetraisopropyldisiloxanyl-β-D-ribofuranosyl)-2-diphenylcarbamoyloxyimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 83-01-2
diphenylcarbamic chloride

: 793674-23-4
1-(2-deoxy-3,5-di-O-tetraisopropyldisiloxanyl-β-D-ribofuranosyl)imidazolin-2-one

: 793674-24-5
1-(2-deoxy-3,5-di-O-tetraisopropyldisiloxanyl-β-D-ribofuranosyl)-2-diphenylcarbamoyloxyimidazole

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In pyridine; at 20 ℃; for 12h;
DOI:10.1021/ja047201d

Reference yield:

: 500778-10-9
1-(2-deoxy-β-D-ribofuranosyl)imidazolin-2-one

: 793674-24-5
1-(2-deoxy-3,5-di-O-tetraisopropyldisiloxanyl-β-D-ribofuranosyl)-2-diphenylcarbamoyloxyimidazole

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / pyridine / dimethylformamide / 12 h / 20 °C

2: 60 percent / N,N-diisopropylethylamine / pyridine / 12 h / 20 °C

With pyridine; N-ethyl-N,N-diisopropylamine; In pyridine; N,N-dimethyl-formamide;
DOI:10.1021/ja047201d