C₄₄H₅₈O₅S₃Si

Base Information

Chemical Name:C₄₄H₅₈O₅S₃Si
CAS No.:90344-14-2
Molecular Formula:C₄₄H₅₈O₅S₃Si
Molecular Weight:791.225
Hs Code.:

C<sub>44</sub>H<sub>58</sub>O<sub>5</sub>S<sub>3</sub>Si

Synonyms:C₄₄H₅₈O₅S₃Si

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Chemical Property of C₄₄H₅₈O₅S₃Si

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Technology Process of C₄₄H₅₈O₅S₃Si

There total 16 articles about C₄₄H₅₈O₅S₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 80106-30-5
(4E,6E)-octa-4,6-dien-1-ol

: 90344-14-2
C₄₄H₅₈O₅S₃Si

Guidance literature:: Multi-step reaction with 14 steps

1: 95 percent / pyridine / 15 h / 5 °C

2: 94 percent / NaOMe / methanol / 2 h

3: 75 percent / 40 percent peracetic acid / ethyl acetate / 2 h / -20 - 0 °C

4: 70 percent / benzene / 24 h / 80 °C

5: 1 M lithium bis(trimethylsilyl)amide / tetrahydrofuran / -78 deg C, 5 d, -40 deg C, 8 h

7: aluminum amalgam / tetrahydrofuran; H₂O / 3 h

8: 92 percent / NaOMe / methanol / 24 h / 40 °C

9: 100 percent / TsOH / benzene / 72 h / 80 °C / Dean-Stark apparatus

10: 91 percent / LiAlH₄ / tetrahydrofuran / 2 h / Ambient temperature

11: Me₃SiCl, NaI / acetonitrile / 1 h

12: benzene / 3 h / 80 °C / dark

13: 100 percent / BF₃*Et₂O / CH₂Cl₂ / 15 h

14: 1.) 1.6 M n-BuLi / 1.) THF, HMPA, 0 deg C, 30 min; 2.) THF, HMPA, -78 deg C to RT, 4 h

With pyridine; peracetic acid; lithium aluminium tetrahydride; n-butyllithium; chloro-trimethyl-silane; aluminium amalgam; boron trifluoride diethyl etherate; sodium methylate; toluene-4-sulfonic acid; sodium iodide; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; acetonitrile; benzene;
DOI:10.1021/ja00325a017

Reference yield:

: 68823-50-7
methyl (4E,6E)-octa-4,6-dienoate

: 90344-14-2
C₄₄H₅₈O₅S₃Si

Guidance literature:: Multi-step reaction with 15 steps

1: 99 percent / LiAlH₄ / tetrahydrofuran / 1 h / 0 °C

2: 95 percent / pyridine / 15 h / 5 °C

3: 94 percent / NaOMe / methanol / 2 h

4: 75 percent / 40 percent peracetic acid / ethyl acetate / 2 h / -20 - 0 °C

5: 70 percent / benzene / 24 h / 80 °C

6: 1 M lithium bis(trimethylsilyl)amide / tetrahydrofuran / -78 deg C, 5 d, -40 deg C, 8 h

8: aluminum amalgam / tetrahydrofuran; H₂O / 3 h

9: 92 percent / NaOMe / methanol / 24 h / 40 °C

10: 100 percent / TsOH / benzene / 72 h / 80 °C / Dean-Stark apparatus

11: 91 percent / LiAlH₄ / tetrahydrofuran / 2 h / Ambient temperature

12: Me₃SiCl, NaI / acetonitrile / 1 h

13: benzene / 3 h / 80 °C / dark

14: 100 percent / BF₃*Et₂O / CH₂Cl₂ / 15 h

15: 1.) 1.6 M n-BuLi / 1.) THF, HMPA, 0 deg C, 30 min; 2.) THF, HMPA, -78 deg C to RT, 4 h

With pyridine; peracetic acid; lithium aluminium tetrahydride; n-butyllithium; chloro-trimethyl-silane; aluminium amalgam; boron trifluoride diethyl etherate; sodium methylate; toluene-4-sulfonic acid; sodium iodide; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; acetonitrile; benzene;
DOI:10.1021/ja00325a017

Reference yield:

: 75283-60-2
dimethyl 2-[(2E,4E)-hexa-2,4-dienyl]propanedioate

: 90344-14-2
C₄₄H₅₈O₅S₃Si

Guidance literature:: Multi-step reaction with 16 steps

1: 75 percent / sodium cyanide / dimethylsulfoxide / 3 h / 120 °C

2: 99 percent / LiAlH₄ / tetrahydrofuran / 1 h / 0 °C

3: 95 percent / pyridine / 15 h / 5 °C

4: 94 percent / NaOMe / methanol / 2 h

5: 75 percent / 40 percent peracetic acid / ethyl acetate / 2 h / -20 - 0 °C

6: 70 percent / benzene / 24 h / 80 °C

7: 1 M lithium bis(trimethylsilyl)amide / tetrahydrofuran / -78 deg C, 5 d, -40 deg C, 8 h

9: aluminum amalgam / tetrahydrofuran; H₂O / 3 h

10: 92 percent / NaOMe / methanol / 24 h / 40 °C

11: 100 percent / TsOH / benzene / 72 h / 80 °C / Dean-Stark apparatus

12: 91 percent / LiAlH₄ / tetrahydrofuran / 2 h / Ambient temperature

13: Me₃SiCl, NaI / acetonitrile / 1 h

14: benzene / 3 h / 80 °C / dark

15: 100 percent / BF₃*Et₂O / CH₂Cl₂ / 15 h

16: 1.) 1.6 M n-BuLi / 1.) THF, HMPA, 0 deg C, 30 min; 2.) THF, HMPA, -78 deg C to RT, 4 h

With pyridine; peracetic acid; sodium cyanide; lithium aluminium tetrahydride; n-butyllithium; chloro-trimethyl-silane; aluminium amalgam; boron trifluoride diethyl etherate; sodium methylate; toluene-4-sulfonic acid; sodium iodide; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; dichloromethane; water; dimethyl sulfoxide; ethyl acetate; acetonitrile; benzene;
DOI:10.1021/ja00325a017