(2S,3S,4R)-2,4-Bis(benzoyloxy)-1,1-bis[(benzoyloxy)methyl]-3-(benzyloxy)cyclohexane

Base Information

Chemical Name:(2S,3S,4R)-2,4-Bis(benzoyloxy)-1,1-bis[(benzoyloxy)methyl]-3-(benzyloxy)cyclohexane
CAS No.:360562-27-2
Molecular Formula:C₄₃H₃₈O₉
Molecular Weight:698.769
Hs Code.:

Synonyms:(2S,3S,4R)-2,4-Bis(benzoyloxy)-1,1-bis[(benzoyloxy)methyl]-3-(benzyloxy)cyclohexane

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Chemical Property of (2S,3S,4R)-2,4-Bis(benzoyloxy)-1,1-bis[(benzoyloxy)methyl]-3-(benzyloxy)cyclohexane

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Technology Process of (2S,3S,4R)-2,4-Bis(benzoyloxy)-1,1-bis[(benzoyloxy)methyl]-3-(benzyloxy)cyclohexane

There total 1 articles about (2S,3S,4R)-2,4-Bis(benzoyloxy)-1,1-bis[(benzoyloxy)methyl]-3-(benzyloxy)cyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 98-88-4
benzoyl chloride

: (1R,2S,3RS)-2-(Benzyloxy)-4,4-bis(hydroxymethyl)cyclohexane-1,3-diol

: 360562-27-2
(2S,3S,4R)-2,4-Bis(benzoyloxy)-1,1-bis[(benzoyloxy)methyl]-3-(benzyloxy)cyclohexane

: (2R,3S,4R)-2,4-Bis(benzoyloxy)-1,1-bis[(benzoyloxy)methyl]-3-(benzyloxy)cyclohexane

Guidance literature:: With pyridine; at 20 ℃; for 48h;
DOI:10.1135/cccc20010785

Reference yield: 95.0%

: 360562-27-2
(2S,3S,4R)-2,4-Bis(benzoyloxy)-1,1-bis[(benzoyloxy)methyl]-3-(benzyloxy)cyclohexane

: 360562-29-4
(1S,2S,6R)-2,6-Bis(benzoyloxy)-3,3-bis[(benzoyloxy)methyl]cyclohexan-1-ol

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide; for 50h;
DOI:10.1135/cccc20010785

Reference yield:

: 360562-27-2
(2S,3S,4R)-2,4-Bis(benzoyloxy)-1,1-bis[(benzoyloxy)methyl]-3-(benzyloxy)cyclohexane

: 360562-31-8
(2R,4R)-2,4-Bis(benzoyloxy)-1,1-bis[(benzoyloxy)methyl]cyclohexane

Guidance literature:: Multi-step reaction with 3 steps

1.1: 95 percent / H₂ / 10 percent Pd/C / methanol; dimethylformamide / 50 h

2.1: NaH / dimethylformamide / 0.5 h / 0 °C

2.2: 79 percent / dimethylformamide / 1 h / 0 - 20 °C

3.1: 95 percent / Bu₃SnH; AIBN / toluene / 0.5 h / Heating

With 2,2'-azobis(isobutyronitrile); hydrogen; tri-n-butyl-tin hydride; sodium hydride; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide; toluene;
DOI:10.1135/cccc20010785