1-(N⁶-benzoyl-5'-deoxy-adenosin-5'-yl)-2-methyl-3-phenylsulfonyl-isothiourea

Base Information

Chemical Name:1-(N⁶-benzoyl-5'-deoxy-adenosin-5'-yl)-2-methyl-3-phenylsulfonyl-isothiourea
CAS No.:162757-19-9
Molecular Formula:C₂₅H₂₅N₇O₆S₂
Molecular Weight:583.649
Hs Code.:

1-(N<sup>6</sup>-benzoyl-5'-deoxy-adenosin-5'-yl)-2-methyl-3-phenylsulfonyl-isothiourea

Synonyms:1-(N⁶-benzoyl-5'-deoxy-adenosin-5'-yl)-2-methyl-3-phenylsulfonyl-isothiourea

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Chemical Property of 1-(N⁶-benzoyl-5'-deoxy-adenosin-5'-yl)-2-methyl-3-phenylsulfonyl-isothiourea

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Technology Process of 1-(N⁶-benzoyl-5'-deoxy-adenosin-5'-yl)-2-methyl-3-phenylsulfonyl-isothiourea

There total 9 articles about 1-(N⁶-benzoyl-5'-deoxy-adenosin-5'-yl)-2-methyl-3-phenylsulfonyl-isothiourea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 21950-36-7
5'-amino-5'-deoxy-2',3'-O-isopropylideneadenosine

: 162757-19-9
1-(N⁶-benzoyl-5'-deoxy-adenosin-5'-yl)-2-methyl-3-phenylsulfonyl-isothiourea

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / pyridine / 4 h / 80 °C

2: 97 percent / pyridine / 2 h / Ambient temperature

3: 71 percent / CF₃CO₃₂H / H₂O / 0.67 h / Ambient temperature

With pyridine; C₂⁽²⁾HF₃O₃; In pyridine; water;
DOI:10.1080/15257779508014657

Reference yield:

: 68144-26-3
5'-azido-5'-deoxy-N⁶-benzoyl-2',3'-O-isopropylidene adenosine

: 162757-19-9
1-(N⁶-benzoyl-5'-deoxy-adenosin-5'-yl)-2-methyl-3-phenylsulfonyl-isothiourea

Guidance literature:: Multi-step reaction with 5 steps

1: 66 percent / NH₃, MeOH / 40 h / Ambient temperature

2: 70 percent / H₂ / Pd-C / ethanol / 5 h / 2327.2 Torr

3: 93 percent / pyridine / 4 h / 80 °C

4: 97 percent / pyridine / 2 h / Ambient temperature

5: 71 percent / CF₃CO₃₂H / H₂O / 0.67 h / Ambient temperature

With pyridine; methanol; C₂⁽²⁾HF₃O₃; ammonia; hydrogen; palladium on activated charcoal; In pyridine; ethanol; water;
DOI:10.1080/15257779508014657

Reference yield:

: 68179-90-8,7687-45-8
((3aR,4R,6R,6aR)-6-(6-amino-9H-purin-9-yl)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)methyl methanesulfonate

: 162757-19-9
1-(N⁶-benzoyl-5'-deoxy-adenosin-5'-yl)-2-methyl-3-phenylsulfonyl-isothiourea

Guidance literature:: Multi-step reaction with 8 steps

1: Ambient temperature

2: 88 percent / NH₃/EtOH / 1.5 h

3: 84 percent / NaN₃ / dimethylformamide / 45 h / 80 °C

4: 66 percent / NH₃, MeOH / 40 h / Ambient temperature

5: 70 percent / H₂ / Pd-C / ethanol / 5 h / 2327.2 Torr

6: 93 percent / pyridine / 4 h / 80 °C

7: 97 percent / pyridine / 2 h / Ambient temperature

8: 71 percent / CF₃CO₃₂H / H₂O / 0.67 h / Ambient temperature

With pyridine; methanol; sodium azide; ethanol; C₂⁽²⁾HF₃O₃; ammonia; hydrogen; palladium on activated charcoal; In pyridine; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1080/15257779508014657