C₁₉H₁₆BrFN₂*ClH

Base Information

Chemical Name:C₁₉H₁₆BrFN₂*ClH
CAS No.:1273523-86-6
Molecular Formula:C₁₉H₁₆BrFN₂*ClH
Molecular Weight:407.713
Hs Code.:

C<sub>19</sub>H<sub>16</sub>BrFN<sub>2</sub>*ClH

Synonyms:C₁₉H₁₆BrFN₂*ClH

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Chemical Property of C₁₉H₁₆BrFN₂*ClH

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Technology Process of C₁₉H₁₆BrFN₂*ClH

There total 3 articles about C₁₉H₁₆BrFN₂*ClH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 41979-39-9
4-piperidone hydrochloride

: 138900-24-0
1-(4-fluorophenyl)-5-bromo-1H-indole

: 1273523-86-6
C₁₉H₁₆BrFN₂*ClH

Guidance literature:: 4-piperidone hydrochloride; 1-(4-fluorophenyl)-5-bromo-1H-indole; With trifluoroacetic acid; In water; acetic acid; at 100 - 105 ℃; for 1h;

With hydrogenchloride; In water; acetic acid; at 20 ℃;
DOI:10.3762/bjoc.7.5

Reference yield:

: 10075-50-0
5-bromo-1H-indole

: 1273523-86-6
C₁₉H₁₆BrFN₂*ClH

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate; ethylenediamine; copper(I) bromide / N,N-dimethyl-formamide / 48 h / 130 - 135 °C / Inert atmosphere

2.1: trifluoroacetic acid / water; acetic acid / 1 h / 100 - 105 °C

2.2: 20 °C

With potassium carbonate; ethylenediamine; trifluoroacetic acid; copper(I) bromide; In water; acetic acid; N,N-dimethyl-formamide;
DOI:10.3762/bjoc.7.5

Reference yield:

: 460-00-4
1-Bromo-4-fluorobenzene

: 1273523-86-6
C₁₉H₁₆BrFN₂*ClH

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate; ethylenediamine; copper(I) bromide / N,N-dimethyl-formamide / 48 h / 130 - 135 °C / Inert atmosphere

2.1: trifluoroacetic acid / water; acetic acid / 1 h / 100 - 105 °C

2.2: 20 °C

With potassium carbonate; ethylenediamine; trifluoroacetic acid; copper(I) bromide; In water; acetic acid; N,N-dimethyl-formamide;
DOI:10.3762/bjoc.7.5