C₇₉H₁₂₉N₃O₉S

Base Information

• Chemical Name: C₇₉H₁₂₉N₃O₉S
• CAS No.: 1324007-72-8
• Molecular Formula: C₇₉H₁₂₉N₃O₉S
• Molecular Weight: 1296.97
• Mol file: 1324007-72-8.mol

Synonyms:C₇₉H₁₂₉N₃O₉S

Chemical Property of C₇₉H₁₂₉N₃O₉S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₇₉H₁₂₉N₃O₉S

There total 6 articles about C₇₉H₁₂₉N₃O₉S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl 2,4-di(docosyloxy)benzoate → C79H129N3O9S (1324007-72-8)

Guidance literature:

Multi-step reaction with 4 steps

1: lithium aluminium tetrahydride / tetrahydrofuran

2: dmap; diisopropyl-carbodiimide / dichloromethane / 20 °C

3: piperidine; 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 20 °C

4: benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 °C

With piperidine; dmap; lithium aluminium tetrahydride; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; diisopropyl-carbodiimide; In tetrahydrofuran; dichloromethane;

DOI:10.1016/j.bmcl.2011.06.004

Reference yield:

1-Bromodocosane (6938-66-5) → C79H129N3O9S (1324007-72-8)

Guidance literature:

Multi-step reaction with 5 steps

1: desipramine; potassium carbonate

2: lithium aluminium tetrahydride / tetrahydrofuran

3: dmap; diisopropyl-carbodiimide / dichloromethane / 20 °C

4: piperidine; 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 20 °C

5: benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 °C

With piperidine; dmap; lithium aluminium tetrahydride; desipramine; potassium carbonate; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; diisopropyl-carbodiimide; In tetrahydrofuran; dichloromethane;

DOI:10.1016/j.bmcl.2011.06.004

Reference yield:

methyl 2,4-dihydroxybenzoate (2150-47-2) → C79H129N3O9S (1324007-72-8)

Guidance literature:

Multi-step reaction with 5 steps

1: desipramine; potassium carbonate

2: lithium aluminium tetrahydride / tetrahydrofuran

3: dmap; diisopropyl-carbodiimide / dichloromethane / 20 °C

4: piperidine; 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 20 °C

5: benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 °C

With piperidine; dmap; lithium aluminium tetrahydride; desipramine; potassium carbonate; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; diisopropyl-carbodiimide; In tetrahydrofuran; dichloromethane;

DOI:10.1016/j.bmcl.2011.06.004

upstream raw materials:

2,4-bis(docosyloxy)benzyl alcohol

C₇₂H₁₁₆N₂O₇S

1-Bromodocosane

methyl 2,4-dihydroxybenzoate

Downstream raw materials:

C₆₄H₁₁₉N₃O₇S