C₂₇H₄₁NO₆S

Base Information

Chemical Name:C₂₇H₄₁NO₆S
CAS No.:931581-18-9
Molecular Formula:C₂₇H₄₁NO₆S
Molecular Weight:507.692
Hs Code.:

C<sub>27</sub>H<sub>41</sub>NO<sub>6</sub>S

Synonyms:C₂₇H₄₁NO₆S

Suppliers and Price of C₂₇H₄₁NO₆S

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₇H₄₁NO₆S

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₇H₄₁NO₆S

There total 1 articles about C₂₇H₄₁NO₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 125664-97-3
1-((3aS,6R,7aR)-8,8-dimethyl-2,2-dioxidohexahydro-1H-3a,6-methanobenzo[c]isothiazol-1-yl)hexan-1-one

: 126361-27-1
(S)-(p-methoxybenzyloxy)propanal

: 931581-18-9
C₂₇H₄₁NO₆S

Guidance literature:: 1-((3aS,6R,7aR)-8,8-dimethyl-2,2-dioxidohexahydro-1H-3a,6-methanobenzo[c]isothiazol-1-yl)hexan-1-one; With di-n-butylboryl trifluoromethanesulfonate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at -5 ℃; for 0.5h;

(S)-(p-methoxybenzyloxy)propanal; In dichloromethane; at -78 ℃; for 1h; stereoselective reaction;
DOI:10.1002/ejoc.201100034

Reference yield: 74.0%

: 931581-18-9
C₂₇H₄₁NO₆S

: 107-18-6
allyl alcohol

: 931581-19-0
C₂₀H₃₀O₅

Guidance literature:: With titanium(IV) isopropylate; at 150 ℃; for 48h; Molecular sieve;
DOI:10.1002/ejoc.201100034

Reference yield:

: 931581-18-9
C₂₇H₄₁NO₆S

: 896434-12-1
3-Methyl-butyric acid (2R,3S,6S,7R,8R)-3-(2-benzyloxy-3-formylamino-benzoylamino)-8-butyl-2,6-dimethyl-4,9-dioxo-[1,5]dioxonan-7-yl ester

Guidance literature:: Multi-step reaction with 12 steps

1: titanium(IV) isopropylate / 48 h / 150 °C / Molecular sieve

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 4 h / 0 - 20 °C

3: water; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 0.5 h / 20 °C

4: dmap; triethylamine / toluene / 16 h / 0 - 20 °C

5: hydrogenchloride; water / ethanol / 24 h / 20 °C

6: pyrrolidine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triphenylphosphine / acetonitrile / 7 h / 0 - 20 °C

7: triphenylphosphine / toluene / 3 h / 20 °C

8: copper(I) trifluoromethanesulfonate benzene / benzene / 3 h / 80 °C

9: pyridine hydrogenfluoride / tetrahydrofuran / 3 h / 20 °C

10: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C

11: palladium on carbon; hydrogen / tetrahydrofuran / 2 h / 20 °C / 760.05 Torr / Darkness

12: 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 24 h / 20 °C

With pyrrolidine; 4-methyl-morpholine; titanium(IV) isopropylate; hydrogenchloride; dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(I) trifluoromethanesulfonate benzene; palladium on carbon; water; hydrogen; benzotriazol-1-ol; pyridine hydrogenfluoride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile; benzene;
DOI:10.1002/ejoc.201100034