Technology Process of C17H16O2
There total 12 articles about C17H16O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogenchloride;
In
tetrahydrofuran; water;
at 0 - 20 ℃;
for 24h;
DOI:10.1055/s-0033-1339484
- Guidance literature:
-
Multi-step reaction with 7 steps
1: Dess-Martin periodane; sodium hydrogencarbonate / dichloromethane / 3 h / 0 - 20 °C
2: tetrahydrofuran / 1 h / 0 - 20 °C
3: Dess-Martin periodane; sodium hydrogencarbonate / dichloromethane / 0.5 h / 0 - 20 °C
4: tetrabutyl ammonium fluoride / tetrahydrofuran / 12 h / 0 - 20 °C
5: 3-chloro-benzenecarboperoxoic acid; scandium tris(trifluoromethanesulfonate) / dichloromethane / 72 h / 0 - 20 °C / Inert atmosphere
6: Dess-Martin periodane; sodium hydrogencarbonate / dichloromethane / 2.5 h / 0 - 20 °C
7: hydrogenchloride / tetrahydrofuran; water / 24 h / 0 - 20 °C
With
hydrogenchloride; tetrabutyl ammonium fluoride; sodium hydrogencarbonate; Dess-Martin periodane; 3-chloro-benzenecarboperoxoic acid; scandium tris(trifluoromethanesulfonate);
In
tetrahydrofuran; dichloromethane; water;
5: |Baeyer-Villiger Ketone Oxidation;
DOI:10.1055/s-0033-1339484
- Guidance literature:
-
Multi-step reaction with 8 steps
1: lithium borohydride / tetrahydrofuran / 20 h / 0 - 50 °C / Inert atmosphere
2: Dess-Martin periodane; sodium hydrogencarbonate / dichloromethane / 3 h / 0 - 20 °C
3: tetrahydrofuran / 1 h / 0 - 20 °C
4: Dess-Martin periodane; sodium hydrogencarbonate / dichloromethane / 0.5 h / 0 - 20 °C
5: tetrabutyl ammonium fluoride / tetrahydrofuran / 12 h / 0 - 20 °C
6: 3-chloro-benzenecarboperoxoic acid; scandium tris(trifluoromethanesulfonate) / dichloromethane / 72 h / 0 - 20 °C / Inert atmosphere
7: Dess-Martin periodane; sodium hydrogencarbonate / dichloromethane / 2.5 h / 0 - 20 °C
8: hydrogenchloride / tetrahydrofuran; water / 24 h / 0 - 20 °C
With
hydrogenchloride; lithium borohydride; tetrabutyl ammonium fluoride; sodium hydrogencarbonate; Dess-Martin periodane; 3-chloro-benzenecarboperoxoic acid; scandium tris(trifluoromethanesulfonate);
In
tetrahydrofuran; dichloromethane; water;
6: |Baeyer-Villiger Ketone Oxidation;
DOI:10.1055/s-0033-1339484