2-(p-methylphenylaminosulfonylmethyl)-5-(3'-(p-methylphenylsulfonyl)-4',5'-dihydro-1'H-pyrazol-4'-ylsulfonylmethyl)-1,3,4-oxadiazole

Base Information

Chemical Name:2-(p-methylphenylaminosulfonylmethyl)-5-(3'-(p-methylphenylsulfonyl)-4',5'-dihydro-1'H-pyrazol-4'-ylsulfonylmethyl)-1,3,4-oxadiazole
CAS No.:1394128-78-9
Molecular Formula:C₂₁H₂₃N₅O₇S₃
Molecular Weight:553.641
Hs Code.:

Synonyms:2-(p-methylphenylaminosulfonylmethyl)-5-(3'-(p-methylphenylsulfonyl)-4',5'-dihydro-1'H-pyrazol-4'-ylsulfonylmethyl)-1,3,4-oxadiazole

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Chemical Property of 2-(p-methylphenylaminosulfonylmethyl)-5-(3'-(p-methylphenylsulfonyl)-4',5'-dihydro-1'H-pyrazol-4'-ylsulfonylmethyl)-1,3,4-oxadiazole

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Technology Process of 2-(p-methylphenylaminosulfonylmethyl)-5-(3'-(p-methylphenylsulfonyl)-4',5'-dihydro-1'H-pyrazol-4'-ylsulfonylmethyl)-1,3,4-oxadiazole

There total 3 articles about 2-(p-methylphenylaminosulfonylmethyl)-5-(3'-(p-methylphenylsulfonyl)-4',5'-dihydro-1'H-pyrazol-4'-ylsulfonylmethyl)-1,3,4-oxadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 1394128-60-9
2-(p-methylphenylaminosulfonylmethyl)-5-[E-(2-(p-methylphenylsulfonyl)vinyl-sulfonylmethyl)]-1,3,4-oxadiazole

: 1394128-78-9
2-(p-methylphenylaminosulfonylmethyl)-5-(3'-(p-methylphenylsulfonyl)-4',5'-dihydro-1'H-pyrazol-4'-ylsulfonylmethyl)-1,3,4-oxadiazole

Guidance literature:: In diethyl ether; dichloromethane; at -20 - -15 ℃; for 48h;
DOI:10.1016/j.ejmech.2012.06.014

Reference yield:

: 1155273-86-1
(E)-(4-methylphenyl)sulfonylethenesulfonylacetic acid

: 1394128-78-9
2-(p-methylphenylaminosulfonylmethyl)-5-(3'-(p-methylphenylsulfonyl)-4',5'-dihydro-1'H-pyrazol-4'-ylsulfonylmethyl)-1,3,4-oxadiazole

Guidance literature:: Multi-step reaction with 2 steps

1: trichlorophosphate / Reflux

2: diethyl ether; dichloromethane / 48 h / -20 - -15 °C

With trichlorophosphate; In diethyl ether; dichloromethane;
DOI:10.1016/j.ejmech.2012.06.014

Reference yield:

: 1370346-31-8
C₉H₁₃N₃O₃S

: 1394128-78-9
2-(p-methylphenylaminosulfonylmethyl)-5-(3'-(p-methylphenylsulfonyl)-4',5'-dihydro-1'H-pyrazol-4'-ylsulfonylmethyl)-1,3,4-oxadiazole

Guidance literature:: Multi-step reaction with 2 steps

1: trichlorophosphate / Reflux

2: diethyl ether; dichloromethane / 48 h / -20 - -15 °C

With trichlorophosphate; In diethyl ether; dichloromethane;
DOI:10.1016/j.ejmech.2012.06.014