2-(p-methylphenylaminosulfonylmethyl)-5-[E-(2-(p-methylphenylsulfonyl)vinyl-sulfonylmethyl)]-1,3,4-oxadiazole

Base Information

• Chemical Name: 2-(p-methylphenylaminosulfonylmethyl)-5-[E-(2-(p-methylphenylsulfonyl)vinyl-sulfonylmethyl)]-1,3,4-oxadiazole
• CAS No.: 1394128-60-9
• Molecular Formula: C₂₀H₂₁N₃O₇S₃
• Molecular Weight: 511.601

Synonyms:2-(p-methylphenylaminosulfonylmethyl)-5-[E-(2-(p-methylphenylsulfonyl)vinyl-sulfonylmethyl)]-1,3,4-oxadiazole

Chemical Property of 2-(p-methylphenylaminosulfonylmethyl)-5-[E-(2-(p-methylphenylsulfonyl)vinyl-sulfonylmethyl)]-1,3,4-oxadiazole

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Technology Process of 2-(p-methylphenylaminosulfonylmethyl)-5-[E-(2-(p-methylphenylsulfonyl)vinyl-sulfonylmethyl)]-1,3,4-oxadiazole

There total 1 articles about 2-(p-methylphenylaminosulfonylmethyl)-5-[E-(2-(p-methylphenylsulfonyl)vinyl-sulfonylmethyl)]-1,3,4-oxadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

(E)-(4-methylphenyl)sulfonylethenesulfonylacetic acid (1155273-86-1) + C9H13N3O3S (1370346-31-8) → 2-(p-methylphenylaminosulfonylmethyl)-5-[E-(2-(p-methylphenylsulfonyl)vinyl-sulfonylmethyl)]-1,3,4-oxadiazole (1394128-60-9)

Guidance literature:

With trichlorophosphate; Reflux;

DOI:10.1016/j.ejmech.2012.06.014

Reference yield: 66.0%

2-(p-methylphenylaminosulfonylmethyl)-5-[E-(2-(p-methylphenylsulfonyl)vinyl-sulfonylmethyl)]-1,3,4-oxadiazole (1394128-60-9) → 4-amino-3-(p-methylphenylaminosulfonylmethyl)-5-[E-(2-(p-methylphenyl-sulfonyl)vinylsulfonylmethyl)]-1,2,4-triazole (1394128-66-5)

Guidance literature:

With hydrazine hydrate; In butan-1-ol; Reflux;

DOI:10.1016/j.ejmech.2012.06.014

Reference yield: 66.0%

diazomethane (186581-53-3,908094-01-9,334-88-3) + 2-(p-methylphenylaminosulfonylmethyl)-5-[E-(2-(p-methylphenylsulfonyl)vinyl-sulfonylmethyl)]-1,3,4-oxadiazole (1394128-60-9) → 2-(p-methylphenylaminosulfonylmethyl)-5-(3'-(p-methylphenylsulfonyl)-4',5'-dihydro-1'H-pyrazol-4'-ylsulfonylmethyl)-1,3,4-oxadiazole (1394128-78-9)

Guidance literature:

In diethyl ether; dichloromethane; at -20 - -15 ℃; for 48h;

DOI:10.1016/j.ejmech.2012.06.014

upstream raw materials:

(E)-(4-methylphenyl)sulfonylethenesulfonylacetic acid

C₉H₁₃N₃O₃S

Downstream raw materials:

2-(p-methylphenylaminosulfonylmethyl)-5-(3'-(p-methylphenylsulfonyl)-4',5'-dihydro-1'H-pyrazol-4'-ylsulfonylmethyl)-1,3,4-oxadiazole

2-(p-methylphenylaminosulfonylmethyl)-5-[E-(2-(p-methylphenylsulfonyl)vinylsulfonylmethyl)]-1,3,4-thiadiazole

4-amino-3-(p-methylphenylaminosulfonylmethyl)-5-[E-(2-(p-methylphenyl-sulfonyl)vinylsulfonylmethyl)]-1,2,4-triazole

2-(p-methylphenylaminosulfonylmethyl)-5-(4'-(p-methylphenylsulfonyl)-1'H-pyrrol-3'-ylsulfonylmethyl)-1,3,4-oxadiazole

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