O₂-(2,4-dinitro-5-fluorophenyl) 1-(N,N-diethylamino)diazen-1-ium-1,2-diolate

Base Information

• Chemical Name: O₂-(2,4-dinitro-5-fluorophenyl) 1-(N,N-diethylamino)diazen-1-ium-1,2-diolate
• CAS No.: 1093078-06-8
• Molecular Formula: C₁₀H₁₂FN₅O₆
• Molecular Weight: 317.234

Synonyms:O₂-(2,4-dinitro-5-fluorophenyl) 1-(N,N-diethylamino)diazen-1-ium-1,2-diolate

Chemical Property of O₂-(2,4-dinitro-5-fluorophenyl) 1-(N,N-diethylamino)diazen-1-ium-1,2-diolate

Chemical Property:

Purity/Quality:

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Technology Process of O₂-(2,4-dinitro-5-fluorophenyl) 1-(N,N-diethylamino)diazen-1-ium-1,2-diolate

There total 1 articles about O₂-(2,4-dinitro-5-fluorophenyl) 1-(N,N-diethylamino)diazen-1-ium-1,2-diolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

1,5-difluoro-2,4-dinitrobenzene (327-92-4) + sodium N,N-(diethylamino)diazen-1-ium-1,2-diolate (138475-09-9) → O2-(2,4-dinitro-5-fluorophenyl) 1-(N,N-diethylamino)diazen-1-ium-1,2-diolate (1093078-06-8)

Guidance literature:

With sodium hydrogencarbonate; In tert-butyl alcohol; at 20 ℃;

DOI:10.1021/jm800831y

Reference yield: 90.0%

O2-(2,4-dinitro-5-fluorophenyl) 1-(N,N-diethylamino)diazen-1-ium-1,2-diolate (1093078-06-8) + sodium 1-(4-N,N-diethylcarbamoylpiperazin-1-yl)diazen-1-ium-1,2-diolate (1093078-00-2) → 1-[1-(N,N-diethylamino)diazen-1-ium-1,2-diol-2-ato]-2,4-dinitro-5-{[4-(N,N-diethyl-aminocarbonyl)piperazin-1-yl]diazen-1-ium-1,2-diol-2-ato}benzene (1093077-94-1)

Guidance literature:

In acetone; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1021/jm800831y

Reference yield: 87.0%

(S)-1-[2-(hydroxymethyl)pyrrolidin-1-yl]diazen-1-ium-1,2-diolate sodium salt (949888-30-6,1177456-95-9) + O2-(2,4-dinitro-5-fluorophenyl) 1-(N,N-diethylamino)diazen-1-ium-1,2-diolate (1093078-06-8) → 1-[1-(N,N-diethylamino)diazen-1-ium-1,2-diol-2-ato]-2,4-dinitro-5-{[(2-hydroxymethyl)-pyrrolidin-1-yl]diazen-1-ium-1,2-diol-2-ato}benzene (1093077-95-2)

Guidance literature:

In acetone; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1021/jm800831y

upstream raw materials:

1,5-difluoro-2,4-dinitrobenzene

sodium N,N-(diethylamino)diazen-1-ium-1,2-diolate

Downstream raw materials:

1-[1-(N,N-diethylamino)diazen-1-ium-1,2-diol-2-ato]-2,4-dinitro-5-{[(4-ethoxycarbonyl)piperazin-1-yl]diazen-1-ium-1,2-diol-2-ato}benzene

1-[1-(N,N-diethylamino)diazen-1-ium-1,2-diol-2-ato]-2,4-dinitro-5-{[(2-hydroxymethyl)-pyrrolidin-1-yl]diazen-1-ium-1,2-diol-2-ato}benzene

1-[1-(N,N-diethylamino)diazen-1-ium-1,2-diol-2-ato]-2,4-dinitro-5-{[4-(N,N-diethyl-aminocarbonyl)piperazin-1-yl]diazen-1-ium-1,2-diol-2-ato}benzene

C₄₉H₇₄N₆O₁₅

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