C₂₈H₄₀NO₉P

Base Information

Chemical Name:C₂₈H₄₀NO₉P
CAS No.:1188441-16-8
Molecular Formula:C₂₈H₄₀NO₉P
Molecular Weight:565.601
Hs Code.:

C<sub>28</sub>H<sub>40</sub>NO<sub>9</sub>P

Synonyms:C₂₈H₄₀NO₉P

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Chemical Property of C₂₈H₄₀NO₉P

Chemical Property:

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Technology Process of C₂₈H₄₀NO₉P

There total 11 articles about C₂₈H₄₀NO₉P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.6%

: 1228350-25-1
C₄₂H₅₂NO₉P

: 1188441-16-8
C₂₈H₄₀NO₉P

Guidance literature:: With 5% Pd(II)/C(eggshell); hydrogen; In tetrahydrofuran; at 20 ℃; for 5h; under 1535.79 Torr;
DOI:10.1021/op100063h

Reference yield:

: 1188391-13-0
C₄₂H₅₀NO₉P

: 1188441-16-8
C₂₈H₄₀NO₉P

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; at 20 ℃; for 8h; under 2068.65 Torr;
DOI:10.1016/j.bmcl.2009.07.115

Reference yield:

: C₃₆H₄₅NO₆

: 1188441-16-8
C₂₈H₄₀NO₉P

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogenchloride; zinc(II) chloride / 1,4-dioxane; water / 5 h / 10 - 25 °C

2: palladium 10% on activated carbon; hydrogen / tetrahydrofuran / 25 °C / 2250.23 Torr

3: dmap; N-ethyl-N,N-diisopropylamine / tetrachloromethane; acetonitrile / 2.5 h / -25 - -20 °C / Inert atmosphere

4: 5% Pd(II)/C(eggshell); hydrogen / tetrahydrofuran / 5 h / 20 °C / 1535.79 Torr

With hydrogenchloride; dmap; 5% Pd(II)/C(eggshell); palladium 10% on activated carbon; hydrogen; N-ethyl-N,N-diisopropylamine; zinc(II) chloride; In tetrahydrofuran; 1,4-dioxane; tetrachloromethane; water; acetonitrile;
DOI:10.1021/op100063h