C₁₂H₁₃IO₂

Base Information

Chemical Name:C₁₂H₁₃IO₂
CAS No.:1620074-31-8
Molecular Formula:C₁₂H₁₃IO₂
Molecular Weight:316.139
Hs Code.:

C<sub>12</sub>H<sub>13</sub>IO<sub>2</sub>

Synonyms:C₁₂H₁₃IO₂

Suppliers and Price of C₁₂H₁₃IO₂

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₁₂H₁₃IO₂

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₁₂H₁₃IO₂

There total 7 articles about C₁₂H₁₃IO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 1620074-30-7
C₁₂H₁₅NO₂

: 1620074-31-8
C₁₂H₁₃IO₂

Guidance literature:: With toluene-4-sulfonic acid; potassium iodide; sodium nitrite; In water; acetonitrile; at 20 ℃; for 2h;

Reference yield:

: 98480-31-0
(1-(4-bromophenyl)cyclopropyl)methanol

: 1620074-31-8
C₁₂H₁₃IO₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: triethylamine / dichloromethane / 3 h / -78 - 0 °C

2.1: triethylamine / N,N-dimethyl-formamide / 3 h / 70 °C

3.1: sodium hydroxide / methanol; water / 16 h / 60 °C

3.2: pH 3

4.1: hydrogenchloride / 18 h / Reflux

5.1: palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / toluene / 18 h / 110 °C / Inert atmosphere

6.1: sodium nitrite; toluene-4-sulfonic acid; potassium iodide / water; acetonitrile / 2 h / 20 °C

With hydrogenchloride; palladium diacetate; caesium carbonate; toluene-4-sulfonic acid; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; triethylamine; potassium iodide; sodium hydroxide; sodium nitrite; In methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile;

Reference yield:

: 638220-35-6
1-(4-bromophenyl)-cyclopropanecarboxylic acid methyl ester

: 1620074-31-8
C₁₂H₁₃IO₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / -4 °C

2.1: triethylamine / dichloromethane / 3 h / -78 - 0 °C

3.1: triethylamine / N,N-dimethyl-formamide / 3 h / 70 °C

4.1: sodium hydroxide / methanol; water / 16 h / 60 °C

4.2: pH 3

5.1: hydrogenchloride / 18 h / Reflux

6.1: palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / toluene / 18 h / 110 °C / Inert atmosphere

7.1: sodium nitrite; toluene-4-sulfonic acid; potassium iodide / water; acetonitrile / 2 h / 20 °C

With hydrogenchloride; lithium aluminium tetrahydride; palladium diacetate; caesium carbonate; toluene-4-sulfonic acid; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; triethylamine; potassium iodide; sodium hydroxide; sodium nitrite; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile;