(E,E)-1-[4-(methoxymethoxy)styryl]-4-[3,4-di(methoxymethoxy)styryl]benzene

Base Information

Chemical Name:(E,E)-1-[4-(methoxymethoxy)styryl]-4-[3,4-di(methoxymethoxy)styryl]benzene
CAS No.:1256281-32-9
Molecular Formula:C₂₈H₃₀O₆
Molecular Weight:462.543
Hs Code.:

Synonyms:(E,E)-1-[4-(methoxymethoxy)styryl]-4-[3,4-di(methoxymethoxy)styryl]benzene

Suppliers and Price of (E,E)-1-[4-(methoxymethoxy)styryl]-4-[3,4-di(methoxymethoxy)styryl]benzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E,E)-1-[4-(methoxymethoxy)styryl]-4-[3,4-di(methoxymethoxy)styryl]benzene

Chemical Property:

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Technology Process of (E,E)-1-[4-(methoxymethoxy)styryl]-4-[3,4-di(methoxymethoxy)styryl]benzene

There total 7 articles about (E,E)-1-[4-(methoxymethoxy)styryl]-4-[3,4-di(methoxymethoxy)styryl]benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6515-06-6
3,4-bis-methoxymethoxy-benzaldehyde

: C₂₁H₂₇O₅P

: 1256281-32-9
(E,E)-1-[4-(methoxymethoxy)styryl]-4-[3,4-di(methoxymethoxy)styryl]benzene

Guidance literature:: With sodium methylate; In methanol; N,N-dimethyl-formamide; at 80 ℃; for 1h; Inert atmosphere;
DOI:10.1021/jm1006929

Reference yield:

: 220882-37-1
4-(methoxymethoxy)-1-ethynylbenzene

: 1256281-32-9
(E,E)-1-[4-(methoxymethoxy)styryl]-4-[3,4-di(methoxymethoxy)styryl]benzene

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen / ethanol; ethyl acetate / 1 h / 760.05 Torr

2: phenyl carbamate; palladium diacetate; potassium carbonate / N,N-dimethyl-formamide / 22 h / 110 °C / Inert atmosphere

3: sodium methylate / methanol; N,N-dimethyl-formamide / 1 h / 80 °C / Inert atmosphere

With phenyl carbamate; hydrogen; sodium methylate; palladium diacetate; potassium carbonate; In methanol; ethanol; ethyl acetate; N,N-dimethyl-formamide; 2: Heck reaction / 3: Horner-Wadsworth-Emmons olefination;
DOI:10.1021/jm1006929

Reference yield:

: 142357-48-0
1-(methoxymethoxy)-4-vinylbenzene

: 1256281-32-9
(E,E)-1-[4-(methoxymethoxy)styryl]-4-[3,4-di(methoxymethoxy)styryl]benzene

Guidance literature:: Multi-step reaction with 2 steps

1: phenyl carbamate; palladium diacetate; potassium carbonate / N,N-dimethyl-formamide / 22 h / 110 °C / Inert atmosphere

2: sodium methylate / methanol; N,N-dimethyl-formamide / 1 h / 80 °C / Inert atmosphere

With phenyl carbamate; sodium methylate; palladium diacetate; potassium carbonate; In methanol; N,N-dimethyl-formamide; 1: Heck reaction / 2: Horner-Wadsworth-Emmons olefination;
DOI:10.1021/jm1006929