2-O-benzoyl-3,4,6-tri-O-levulinoyl-1-O-trichloroacetoimidoyl-α-D-galactopyranose

Base Information

Chemical Name:2-O-benzoyl-3,4,6-tri-O-levulinoyl-1-O-trichloroacetoimidoyl-α-D-galactopyranose
CAS No.:677767-09-8
Molecular Formula:C₃₀H₃₄Cl₃NO₁₃
Molecular Weight:722.958
Hs Code.:

Synonyms:2-O-benzoyl-3,4,6-tri-O-levulinoyl-1-O-trichloroacetoimidoyl-α-D-galactopyranose

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Chemical Property of 2-O-benzoyl-3,4,6-tri-O-levulinoyl-1-O-trichloroacetoimidoyl-α-D-galactopyranose

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Technology Process of 2-O-benzoyl-3,4,6-tri-O-levulinoyl-1-O-trichloroacetoimidoyl-α-D-galactopyranose

There total 5 articles about 2-O-benzoyl-3,4,6-tri-O-levulinoyl-1-O-trichloroacetoimidoyl-α-D-galactopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 545-06-2
trichloroacetonitrile

: Benzoic acid (2R,3R,4S,5S,6R)-2-hydroxy-4,5-bis-(4-oxo-pentanoyloxy)-6-(4-oxo-pentanoyloxymethyl)-tetrahydro-pyran-3-yl ester

: 677767-09-8
2-O-benzoyl-3,4,6-tri-O-levulinoyl-1-O-trichloroacetoimidoyl-α-D-galactopyranose

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 20 ℃; for 0.5h;
DOI:10.1039/b314244b

Reference yield:

: 123-76-2
levulinic acid

: 677767-09-8
2-O-benzoyl-3,4,6-tri-O-levulinoyl-1-O-trichloroacetoimidoyl-α-D-galactopyranose

Guidance literature:: Multi-step reaction with 3 steps

1: 5.48 g / DMAP; 1,3-dicyclohexylcarbodiimide / CH₂Cl₂ / 2 h

2: 90 percent / aq. cerium(IV) ammonium nitrate / toluene; acetonitrile / 0.25 h / 20 °C

3: 1.31 g / DBU / CH₂Cl₂ / 0.5 h / 20 °C

With dmap; ammonium cerium(IV) nitrate; 1,8-diazabicyclo[5.4.0]undec-7-ene; dicyclohexyl-carbodiimide; In dichloromethane; toluene; acetonitrile;
DOI:10.1039/b314244b

Reference yield:

: 671194-40-4
4-methoxyphenyl 2-O-benzoyl-4,6-O-benzylidene-β-D-galactopyranoside

: 677767-09-8
2-O-benzoyl-3,4,6-tri-O-levulinoyl-1-O-trichloroacetoimidoyl-α-D-galactopyranose

Guidance literature:: Multi-step reaction with 4 steps

1: aq. CF₃COOH / 0.25 h / 20 °C

2: 5.48 g / DMAP; 1,3-dicyclohexylcarbodiimide / CH₂Cl₂ / 2 h

3: 90 percent / aq. cerium(IV) ammonium nitrate / toluene; acetonitrile / 0.25 h / 20 °C

4: 1.31 g / DBU / CH₂Cl₂ / 0.5 h / 20 °C

With dmap; ammonium cerium(IV) nitrate; 1,8-diazabicyclo[5.4.0]undec-7-ene; dicyclohexyl-carbodiimide; trifluoroacetic acid; In dichloromethane; toluene; acetonitrile;
DOI:10.1039/b314244b