2-phenyl-4,5-[1,2-dicarba-closo-dodecaborano⁽¹²⁾]-1,3-diselena-2-borolane

Base Information

• Chemical Name: 2-phenyl-4,5-[1,2-dicarba-closo-dodecaborano⁽¹²⁾]-1,3-diselena-2-borolane
• CAS No.: 1344672-56-5
• Molecular Formula: C₈H₁₅B₁₁Se₂
• Molecular Weight: 388.048

Synonyms:2-phenyl-4,5-[1,2-dicarba-closo-dodecaborano⁽¹²⁾]-1,3-diselena-2-borolane

Chemical Property of 2-phenyl-4,5-[1,2-dicarba-closo-dodecaborano⁽¹²⁾]-1,3-diselena-2-borolane

Chemical Property:

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Technology Process of 2-phenyl-4,5-[1,2-dicarba-closo-dodecaborano⁽¹²⁾]-1,3-diselena-2-borolane

There total 2 articles about 2-phenyl-4,5-[1,2-dicarba-closo-dodecaborano⁽¹²⁾]-1,3-diselena-2-borolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C2B10H10(SeSi(CH3)2Se) (1003194-77-1) + phenylborondichloride (873-51-8) → 2-phenyl-4,5-[1,2-dicarba-closo-dodecaborano(12)]-1,3-diselena-2-borolane (1344672-56-5)

Guidance literature:

In ⁽²⁾H₈-toluene; Se-compd. in (D8)toluene cooled to 0°C, PhBCl2 added, stored 24 hat room temp.; volatile removed in vac.;

DOI:10.1002/ejic.201100563

Reference yield:

C2B10H10(SeSi(CH3)2)2 (1229650-12-7) + phenylborondichloride (873-51-8) → 2-phenyl-4,5-[1,2-dicarba-closo-dodecaborano(12)]-1,3-diselena-2-borolane (1344672-56-5)

Guidance literature:

In ⁽²⁾H₈-toluene; Se-compd. in (D8)toluene cooled to 0°C, PhBCl2 added, stored 24 hat room temp.; volatile removed in vac.;

DOI:10.1002/ejic.201100563

Reference yield:

hex-3-yne (928-49-4) + 2-phenyl-4,5-[1,2-dicarba-closo-dodecaborano(12)]-1,3-diselena-2-borolane (1344672-56-5) → triphenylboroxine (3262-89-3) + 3,4,7,8-bis(1,2-dicarba-closo-dodecaborane[1,2])-1,2,5,6-tetraselena-cyclooctane (947326-05-8) + 2,3-[1,2-dicarba-closo-dodecaborano(12)]-5,6-diethyl-7-phenyl-1,4-diselena-7-boracyclohept-3-ene (1403558-83-7)

Guidance literature:

In ⁽²⁾H₈-toluene; at -50 - 50 ℃; for 116h;

DOI:10.1002/ejic.201200471

upstream raw materials:

C₂B₁₀H₁₀(SeSi(CH₃)2Se)

phenylborondichloride

C₂B₁₀H₁₀(SeSi(CH₃)2)2

Downstream raw materials:

triphenylboroxine

3,4,7,8-bis(1,2-dicarba-closo-dodecaborane[1,2])-1,2,5,6-tetraselena-cyclooctane

2,3-[1,2-dicarba-closo-dodecaborano⁽¹²⁾]-5,6-diethyl-7-phenyl-1,4-diselena-7-boracyclohept-3-ene

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