methyl 3,4,6-trideoxy-4-(2,4-di-O-benzoyl-3-deoxy-L-glycero-tetronamido)-2-O-methyl-α-D-mannopyranoside

Base Information

Chemical Name:methyl 3,4,6-trideoxy-4-(2,4-di-O-benzoyl-3-deoxy-L-glycero-tetronamido)-2-O-methyl-α-D-mannopyranoside
CAS No.:208580-01-2
Molecular Formula:C₂₆H₃₁NO₈
Molecular Weight:485.534
Hs Code.:

Synonyms:methyl 3,4,6-trideoxy-4-(2,4-di-O-benzoyl-3-deoxy-L-glycero-tetronamido)-2-O-methyl-α-D-mannopyranoside

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Chemical Property of methyl 3,4,6-trideoxy-4-(2,4-di-O-benzoyl-3-deoxy-L-glycero-tetronamido)-2-O-methyl-α-D-mannopyranoside

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Technology Process of methyl 3,4,6-trideoxy-4-(2,4-di-O-benzoyl-3-deoxy-L-glycero-tetronamido)-2-O-methyl-α-D-mannopyranoside

There total 6 articles about methyl 3,4,6-trideoxy-4-(2,4-di-O-benzoyl-3-deoxy-L-glycero-tetronamido)-2-O-methyl-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 208580-00-1
methyl 3-O-imidazoylthiocarbonyl-4-(2,4-di-O-benzoyl-3-deoxy-L-glycero-tetronamido)-4,6-dideoxy-2-O-methyl-α-D-mannopyranoside

: 208580-01-2
methyl 3,4,6-trideoxy-4-(2,4-di-O-benzoyl-3-deoxy-L-glycero-tetronamido)-2-O-methyl-α-D-mannopyranoside

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; at 110 ℃; for 0.166667h;
DOI:10.1080/07328309808002896

Reference yield:

: 98-88-4
benzoyl chloride

: 208580-01-2
methyl 3,4,6-trideoxy-4-(2,4-di-O-benzoyl-3-deoxy-L-glycero-tetronamido)-2-O-methyl-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / pyridine / CH₂Cl₂ / 2 h / Ambient temperature

2: 100 percent / H₂ / Pd/C / methanol

3: 91 percent / toluene / 6 h / Heating

4: 92 percent / 2,2'-azobis(2-methylpropionitrile), Bu₃SnH / toluene / 0.17 h / 110 °C

With pyridine; 2,2'-azobis(isobutyronitrile); hydrogen; tri-n-butyl-tin hydride; palladium on activated charcoal; In methanol; dichloromethane; toluene;
DOI:10.1080/07328309808002896

Reference yield:

: 178812-81-2
methyl 4-amino-3-O-benzyl-4,6-dideoxy-2-O-methyl-α-D-mannopyranoside

: 208580-01-2
methyl 3,4,6-trideoxy-4-(2,4-di-O-benzoyl-3-deoxy-L-glycero-tetronamido)-2-O-methyl-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 73 percent / pyridine / 100 °C

2: 95 percent / pyridine / CH₂Cl₂ / 2 h / Ambient temperature

3: 100 percent / H₂ / Pd/C / methanol

4: 91 percent / toluene / 6 h / Heating

5: 92 percent / 2,2'-azobis(2-methylpropionitrile), Bu₃SnH / toluene / 0.17 h / 110 °C

With pyridine; 2,2'-azobis(isobutyronitrile); hydrogen; tri-n-butyl-tin hydride; palladium on activated charcoal; In methanol; dichloromethane; toluene;
DOI:10.1080/07328309808002896