(4R,5R)-5-(S)-1-((benzyloxy)-2-((4-methoxybenzyloxy)ethyl)-2,2-dimethyl-1,3-dioxolan-4-yl)methanol

Base Information

Chemical Name:(4R,5R)-5-(S)-1-((benzyloxy)-2-((4-methoxybenzyloxy)ethyl)-2,2-dimethyl-1,3-dioxolan-4-yl)methanol
CAS No.:1423808-53-0
Molecular Formula:C₂₃H₃₀O₆
Molecular Weight:402.488
Hs Code.:

Synonyms:(4R,5R)-5-(S)-1-((benzyloxy)-2-((4-methoxybenzyloxy)ethyl)-2,2-dimethyl-1,3-dioxolan-4-yl)methanol

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Chemical Property of (4R,5R)-5-(S)-1-((benzyloxy)-2-((4-methoxybenzyloxy)ethyl)-2,2-dimethyl-1,3-dioxolan-4-yl)methanol

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Technology Process of (4R,5R)-5-(S)-1-((benzyloxy)-2-((4-methoxybenzyloxy)ethyl)-2,2-dimethyl-1,3-dioxolan-4-yl)methanol

There total 5 articles about (4R,5R)-5-(S)-1-((benzyloxy)-2-((4-methoxybenzyloxy)ethyl)-2,2-dimethyl-1,3-dioxolan-4-yl)methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₃H₂₈O₆

: 1423808-53-0
(4R,5R)-5-(S)-1-((benzyloxy)-2-((4-methoxybenzyloxy)ethyl)-2,2-dimethyl-1,3-dioxolan-4-yl)methanol

Guidance literature:: With sodium tetrahydroborate; In methanol; at 0 - 20 ℃; for 2h;
DOI:10.1016/j.tetlet.2012.12.114

Reference yield:

: 38145-93-6,58846-25-6,73745-56-9
(S)-1-((4R,4'R,5R)-2,2,2',2'-tetramethyl-4,4'-bi(1,3-dioxolan)-5-yl)ethane-1,2-diol

: 1423808-53-0
(4R,5R)-5-(S)-1-((benzyloxy)-2-((4-methoxybenzyloxy)ethyl)-2,2-dimethyl-1,3-dioxolan-4-yl)methanol

Guidance literature:: Multi-step reaction with 4 steps

1.1: di(n-butyl)tin oxide / toluene / 8 h / Reflux

1.2: 12 h / Reflux

2.1: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran / 8 h / 0 - 20 °C

3.1: periodic acid / ethyl acetate / 1 h / 0 - 20 °C

4.1: sodium tetrahydroborate / methanol / 2 h / 0 - 20 °C

With sodium tetrahydroborate; tetra-(n-butyl)ammonium iodide; sodium hydride; di(n-butyl)tin oxide; periodic acid; In tetrahydrofuran; methanol; ethyl acetate; toluene;
DOI:10.1016/j.tetlet.2012.12.114

Reference yield:

: 824-94-2
p-methoxybenzyl chloride

: 1423808-53-0
(4R,5R)-5-(S)-1-((benzyloxy)-2-((4-methoxybenzyloxy)ethyl)-2,2-dimethyl-1,3-dioxolan-4-yl)methanol

Guidance literature:: Multi-step reaction with 4 steps

1.1: di(n-butyl)tin oxide / toluene / 8 h / Reflux

1.2: 12 h / Reflux

2.1: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran / 8 h / 0 - 20 °C

3.1: periodic acid / ethyl acetate / 1 h / 0 - 20 °C

4.1: sodium tetrahydroborate / methanol / 2 h / 0 - 20 °C

With sodium tetrahydroborate; tetra-(n-butyl)ammonium iodide; sodium hydride; di(n-butyl)tin oxide; periodic acid; In tetrahydrofuran; methanol; ethyl acetate; toluene;
DOI:10.1016/j.tetlet.2012.12.114