3--3,4-dihydro-1-phenylnaphthalene hydrochloride

Base Information

Chemical Name:3--3,4-dihydro-1-phenylnaphthalene hydrochloride
CAS No.:80232-36-6
Molecular Formula:C₂₁H₂₃N*ClH
Molecular Weight:325.881
Hs Code.:

3-<N-(cyclopropylmethyl)-N-methylamino>-3,4-dihydro-1-phenylnaphthalene hydrochloride

Synonyms:3--3,4-dihydro-1-phenylnaphthalene hydrochloride

Suppliers and Price of 3--3,4-dihydro-1-phenylnaphthalene hydrochloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3--3,4-dihydro-1-phenylnaphthalene hydrochloride

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3--3,4-dihydro-1-phenylnaphthalene hydrochloride

There total 6 articles about 3--3,4-dihydro-1-phenylnaphthalene hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 345309-45-7
Cyclopropylmethyl-(4-methoxy-4-phenyl-1,2,3,4-tetrahydro-naphthalen-2-yl)-methyl-amine

: 80232-36-6
3--3,4-dihydro-1-phenylnaphthalene hydrochloride

Guidance literature:: With hydrogenchloride; In diethyl ether;
DOI:10.1021/jm00345a005

Reference yield:

: 718-08-1
ethyl 3-oxo-4-phenylbutyrate

: 80232-36-6
3--3,4-dihydro-1-phenylnaphthalene hydrochloride

Guidance literature:: Multi-step reaction with 9 steps

1: methanol / 25 °C

2: NaBH₃CN, HCl gas / methanol

3: pyridine / benzene / 2 h / 25 °C

4: 0.2 N NaOH / tetrahydrofuran / 1 h / 25 °C

5: 41 percent / anhydrous HF / 10 h

6: diethyl ether / 6 h / 25 °C

7: 1.) NaH / 1.) DMF, 2.) DMF, 21 deg C, 10 h

8: LiAlH₄ / diethyl ether / 8 h / 25 °C

9: HCl gas / diethyl ether

With pyridine; hydrogenchloride; sodium hydroxide; lithium aluminium tetrahydride; hydrogen fluoride; sodium hydride; sodium cyanoborohydride; In tetrahydrofuran; methanol; diethyl ether; benzene;
DOI:10.1021/jm00345a005

Reference yield:

: (Z)-3-Methylamino-4-phenyl-but-2-enoic acid ethyl ester

: 80232-36-6
3--3,4-dihydro-1-phenylnaphthalene hydrochloride

Guidance literature:: Multi-step reaction with 8 steps

1: NaBH₃CN, HCl gas / methanol

2: pyridine / benzene / 2 h / 25 °C

3: 0.2 N NaOH / tetrahydrofuran / 1 h / 25 °C

4: 41 percent / anhydrous HF / 10 h

5: diethyl ether / 6 h / 25 °C

6: 1.) NaH / 1.) DMF, 2.) DMF, 21 deg C, 10 h

7: LiAlH₄ / diethyl ether / 8 h / 25 °C

8: HCl gas / diethyl ether

With pyridine; hydrogenchloride; sodium hydroxide; lithium aluminium tetrahydride; hydrogen fluoride; sodium hydride; sodium cyanoborohydride; In tetrahydrofuran; methanol; diethyl ether; benzene;
DOI:10.1021/jm00345a005