C₂₇H₃₀O₆S₂

Base Information

Chemical Name:C₂₇H₃₀O₆S₂
CAS No.:1346433-80-4
Molecular Formula:C₂₇H₃₀O₆S₂
Molecular Weight:514.664
Hs Code.:

C<sub>27</sub>H<sub>30</sub>O<sub>6</sub>S<sub>2</sub>

Synonyms:C₂₇H₃₀O₆S₂

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Chemical Property of C₂₇H₃₀O₆S₂

Chemical Property:

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Technology Process of C₂₇H₃₀O₆S₂

There total 7 articles about C₂₇H₃₀O₆S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 75-15-0,12122-00-8
carbon disulfide

: 1346433-79-1
((2R,3S,4S,5R)-4-benzyloxy-3-(4-methoxybenzyloxy)-5-methyltetrahydrofuran-2-yl)(furan-2-yl)methanol

: 74-88-4
methyl iodide

: 1346433-80-4
C₂₇H₃₀O₆S₂

Guidance literature:: ((2R,3S,4S,5R)-4-benzyloxy-3-(4-methoxybenzyloxy)-5-methyltetrahydrofuran-2-yl)(furan-2-yl)methanol; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 - 20 ℃; for 0.5h; Inert atmosphere;

carbon disulfide; In tetrahydrofuran; mineral oil; at 0 ℃; for 0.5h; Inert atmosphere;

methyl iodide; In tetrahydrofuran; mineral oil; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/jo201570h

Reference yield:

: (3R,4R,5R)-4-(benzyloxy)-5-methyltetrahydro-2,3-furandiol

: 1346433-80-4
C₂₇H₃₀O₆S₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: potassium tert-butylate / dimethyl sulfoxide / 1 h / 0 - 20 °C / Inert atmosphere

1.2: 3 h / 0 - 20 °C / Inert atmosphere

2.1: 1H-imidazole / dichloromethane / 0 °C / Inert atmosphere

3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 - 20 °C / Inert atmosphere

3.2: 20 °C / Inert atmosphere

4.1: camphor-10-sulfonic acid / methanol / 4 h / 0 - 20 °C

5.1: Dess-Martin periodane / dichloromethane / 1 h / 0 °C / Inert atmosphere

6.1: n-butyllithium / diethyl ether; hexane / 1 h / -15 - 20 °C / Inert atmosphere

6.2: 5 h / 0 - 20 °C / Inert atmosphere

7.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 - 20 °C / Inert atmosphere

7.2: 0.5 h / 0 °C / Inert atmosphere

7.3: 0 - 20 °C / Inert atmosphere

With 1H-imidazole; n-butyllithium; camphor-10-sulfonic acid; potassium tert-butylate; sodium hydride; Dess-Martin periodane; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; dimethyl sulfoxide; mineral oil;
DOI:10.1021/jo201570h

Reference yield:

: 1346433-75-7
(3S,4R,5R)-4-benzyloxy-2-(hydroxymethyl)-5-methyltetrahydrofuran-3-ol

: 1346433-80-4
C₂₇H₃₀O₆S₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: 1H-imidazole / dichloromethane / 0 °C / Inert atmosphere

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 - 20 °C / Inert atmosphere

2.2: 20 °C / Inert atmosphere

3.1: camphor-10-sulfonic acid / methanol / 4 h / 0 - 20 °C

4.1: Dess-Martin periodane / dichloromethane / 1 h / 0 °C / Inert atmosphere

5.1: n-butyllithium / diethyl ether; hexane / 1 h / -15 - 20 °C / Inert atmosphere

5.2: 5 h / 0 - 20 °C / Inert atmosphere

6.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 - 20 °C / Inert atmosphere

6.2: 0.5 h / 0 °C / Inert atmosphere

6.3: 0 - 20 °C / Inert atmosphere

With 1H-imidazole; n-butyllithium; camphor-10-sulfonic acid; sodium hydride; Dess-Martin periodane; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; mineral oil;
DOI:10.1021/jo201570h