(+/-)-N-methyl-N-phenyl-2-<2-phenoxy>acetamide

Base Information

Chemical Name:(+/-)-N-methyl-N-phenyl-2-<2-phenoxy>acetamide
CAS No.:237747-91-0
Molecular Formula:C₂₂H₃₀N₂O₂
Molecular Weight:354.492
Hs Code.:

(+/-)-N-methyl-N-phenyl-2-<2-<N-(3-methylhexyl)amino>phenoxy>acetamide

Synonyms:(+/-)-N-methyl-N-phenyl-2-<2-phenoxy>acetamide

Suppliers and Price of (+/-)-N-methyl-N-phenyl-2-<2-phenoxy>acetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-N-methyl-N-phenyl-2-<2-phenoxy>acetamide

Chemical Property:

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Technology Process of (+/-)-N-methyl-N-phenyl-2-<2-phenoxy>acetamide

There total 4 articles about (+/-)-N-methyl-N-phenyl-2-<2-phenoxy>acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 75854-66-9
(+/-)-3-methylhexyl bromide

: 184870-82-4
N-methyl-N-phenyl-2-(2-aminophenoxy)acetamide

: 237747-91-0
(+/-)-N-methyl-N-phenyl-2-<2-phenoxy>acetamide

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 70 ℃; for 48h;
DOI:10.1248/cpb.47.755

Reference yield:

: 1878-87-1
2-nitrophenoxyacetic acid

: 237747-91-0
(+/-)-N-methyl-N-phenyl-2-<2-phenoxy>acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / EDC*HCl, DMAP / CH₂Cl₂ / 72 h / Ambient temperature

2: 91 percent / H₂ / 5 percent Pd/C / methanol / 2.5 h / 760 Torr

3: 54 percent / K₂CO₃ / dimethylformamide / 48 h / 70 °C

With dmap; hydrogen; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium on activated charcoal; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1248/cpb.47.755

Reference yield:

: 100-61-8
N-methylaniline

: 237747-91-0
(+/-)-N-methyl-N-phenyl-2-<2-phenoxy>acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / EDC*HCl, DMAP / CH₂Cl₂ / 72 h / Ambient temperature

2: 91 percent / H₂ / 5 percent Pd/C / methanol / 2.5 h / 760 Torr

3: 54 percent / K₂CO₃ / dimethylformamide / 48 h / 70 °C

With dmap; hydrogen; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium on activated charcoal; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1248/cpb.47.755