4-benzoyloxy-3-bromobenzyl chloride

Base Information

Chemical Name:4-benzoyloxy-3-bromobenzyl chloride
CAS No.:946007-56-3
Molecular Formula:C₁₄H₁₀BrClO₂
Molecular Weight:325.589
Hs Code.:

Synonyms:4-benzoyloxy-3-bromobenzyl chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-benzoyloxy-3-bromobenzyl chloride

Chemical Property:

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Technology Process of 4-benzoyloxy-3-bromobenzyl chloride

There total 4 articles about 4-benzoyloxy-3-bromobenzyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 536974-76-2
3-bromo-4-benzoyloxybenzyl alcohol

: 946007-56-3
4-benzoyloxy-3-bromobenzyl chloride

Guidance literature:: With thionyl chloride; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1021/jm061462b

Reference yield:

: 2973-78-6
3-bromo-4-hydroxybenzylaldehyde

: 946007-56-3
4-benzoyloxy-3-bromobenzyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / Et₃N / ethyl acetate / 5 h / 20 °C

2: 96 percent / NaBH₄ / ethanol / 0 - 20 °C

3: 84 percent / SOCl₂ / CH₂Cl₂ / 2 h / 20 °C

With sodium tetrahydroborate; thionyl chloride; triethylamine; In ethanol; dichloromethane; ethyl acetate;
DOI:10.1021/jm061462b

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 946007-56-3
4-benzoyloxy-3-bromobenzyl chloride

Guidance literature:: Multi-step reaction with 4 steps

1: Br₂; AcOH

2: 89 percent / Et₃N / ethyl acetate / 5 h / 20 °C

3: 96 percent / NaBH₄ / ethanol / 0 - 20 °C

4: 84 percent / SOCl₂ / CH₂Cl₂ / 2 h / 20 °C

With sodium tetrahydroborate; thionyl chloride; bromine; acetic acid; triethylamine; In ethanol; dichloromethane; ethyl acetate;
DOI:10.1021/jm061462b