Methyl 3-O-Benzyl-2,6-dideoxy-4-O-(p-tolylsulfonyl)-α-D-arabino-hexopyranoside

Base Information

Chemical Name:Methyl 3-O-Benzyl-2,6-dideoxy-4-O-(p-tolylsulfonyl)-α-D-arabino-hexopyranoside
CAS No.:121330-33-4
Molecular Formula:C₂₁H₂₆O₆S
Molecular Weight:406.5
Hs Code.:

Synonyms:Methyl 3-O-Benzyl-2,6-dideoxy-4-O-(p-tolylsulfonyl)-α-D-arabino-hexopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methyl 3-O-Benzyl-2,6-dideoxy-4-O-(p-tolylsulfonyl)-α-D-arabino-hexopyranoside

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Technology Process of Methyl 3-O-Benzyl-2,6-dideoxy-4-O-(p-tolylsulfonyl)-α-D-arabino-hexopyranoside

There total 1 articles about Methyl 3-O-Benzyl-2,6-dideoxy-4-O-(p-tolylsulfonyl)-α-D-arabino-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 90762-83-7
Methyl 3-O-benzyl-2,6-dideoxy-α-D-arabino-hexopyranoside

: 98-59-9
p-toluenesulfonyl chloride

: 121330-33-4
Methyl 3-O-Benzyl-2,6-dideoxy-4-O-(p-tolylsulfonyl)-α-D-arabino-hexopyranoside

Guidance literature:: With pyridine; at 55 - 60 ℃; for 13h;
DOI:10.1021/jo00276a015

Reference yield: 90.0%

: 121330-33-4
Methyl 3-O-Benzyl-2,6-dideoxy-4-O-(p-tolylsulfonyl)-α-D-arabino-hexopyranoside

: 14624-27-2
Methyl 2,6-dideoxy-4-O-(p-tolylsulfonyl)-α-D-arabino-hexopyranoside

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 24h; under 760 Torr;
DOI:10.1021/jo00276a015

Reference yield:

: 121330-33-4
Methyl 3-O-Benzyl-2,6-dideoxy-4-O-(p-tolylsulfonyl)-α-D-arabino-hexopyranoside

: 121330-39-0
Methyl 3-O-(3-O-benzyl-2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-4-O-(p-tolylsulfonyl)-α-D-arabino-hexopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / H₂ / 5percent Pd/C / methanol / 24 h / 760 Torr

2: 77 percent / silver silicate / toluene / 12 h

3: 100 percent / NaOH / methanol / 5 h

With sodium hydroxide; silver silicate; hydrogen; palladium on activated charcoal; In methanol; toluene;
DOI:10.1021/jo00276a015