N-allyl-N-{(S)-(5'-tert-butoxycarbonyl-2'-methylphenyl)[(-)-8-phenylmenthyloxycarbonyl]methyl}-N,N-dimethylammonium bromide

Base Information

Chemical Name:N-allyl-N-{(S)-(5'-tert-butoxycarbonyl-2'-methylphenyl)[(-)-8-phenylmenthyloxycarbonyl]methyl}-N,N-dimethylammonium bromide
CAS No.:1088481-56-4
Molecular Formula:Br*C₃₅H₅₀NO₄
Molecular Weight:628.69
Hs Code.:

Synonyms:N-allyl-N-{(S)-(5'-tert-butoxycarbonyl-2'-methylphenyl)[(-)-8-phenylmenthyloxycarbonyl]methyl}-N,N-dimethylammonium bromide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-allyl-N-{(S)-(5'-tert-butoxycarbonyl-2'-methylphenyl)[(-)-8-phenylmenthyloxycarbonyl]methyl}-N,N-dimethylammonium bromide

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Technology Process of N-allyl-N-{(S)-(5'-tert-butoxycarbonyl-2'-methylphenyl)[(-)-8-phenylmenthyloxycarbonyl]methyl}-N,N-dimethylammonium bromide

There total 1 articles about N-allyl-N-{(S)-(5'-tert-butoxycarbonyl-2'-methylphenyl)[(-)-8-phenylmenthyloxycarbonyl]methyl}-N,N-dimethylammonium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1004759-69-6
(2S)-2-(5'-tert-butoxycarbonyl-2'-methylphenyl)-2-(dimethylamino)acetic acid (-)-8-phenylmenthol ester

: 106-95-6
allyl bromide

: 1088481-56-4
N-allyl-N-{(S)-(5'-tert-butoxycarbonyl-2'-methylphenyl)[(-)-8-phenylmenthyloxycarbonyl]methyl}-N,N-dimethylammonium bromide

Guidance literature:: In acetonitrile; at 20 ℃;
DOI:10.1039/b811162f

Reference yield: 91.0%

: 1088481-56-4
N-allyl-N-{(S)-(5'-tert-butoxycarbonyl-2'-methylphenyl)[(-)-8-phenylmenthyloxycarbonyl]methyl}-N,N-dimethylammonium bromide

: 1088481-66-6
(2R)-2-(5'-tert-butoxycarbonyl-2'-methylphenyl)-2-dimethylamino-4-enoic acid (-)-8-phenylmenthol ester

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; at -78 ℃; for 1h; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1039/b811162f