(2R)-2-(5'-tert-butoxycarbonyl-2'-methylphenyl)-2-dimethylamino-4-enoic acid (-)-8-phenylmenthol ester

Base Information

Chemical Name:(2R)-2-(5'-tert-butoxycarbonyl-2'-methylphenyl)-2-dimethylamino-4-enoic acid (-)-8-phenylmenthol ester
CAS No.:1088481-66-6
Molecular Formula:C₃₅H₄₉NO₄
Molecular Weight:547.778
Hs Code.:

Synonyms:(2R)-2-(5'-tert-butoxycarbonyl-2'-methylphenyl)-2-dimethylamino-4-enoic acid (-)-8-phenylmenthol ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R)-2-(5'-tert-butoxycarbonyl-2'-methylphenyl)-2-dimethylamino-4-enoic acid (-)-8-phenylmenthol ester

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Technology Process of (2R)-2-(5'-tert-butoxycarbonyl-2'-methylphenyl)-2-dimethylamino-4-enoic acid (-)-8-phenylmenthol ester

There total 2 articles about (2R)-2-(5'-tert-butoxycarbonyl-2'-methylphenyl)-2-dimethylamino-4-enoic acid (-)-8-phenylmenthol ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1088481-56-4
N-allyl-N-{(S)-(5'-tert-butoxycarbonyl-2'-methylphenyl)[(-)-8-phenylmenthyloxycarbonyl]methyl}-N,N-dimethylammonium bromide

: 1088481-66-6
(2R)-2-(5'-tert-butoxycarbonyl-2'-methylphenyl)-2-dimethylamino-4-enoic acid (-)-8-phenylmenthol ester

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; at -78 ℃; for 1h; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1039/b811162f

Reference yield:

: 1088482-15-8
N-(4'-tert-butoxycarbonylbenzyl)-N,N-dimethyl-N-{1-[(-)-8-phenylmenthyloxycarbonylbut-3-en-1-yl]}ammonium bromide

: 1088481-68-8
(2S)-2-(5'-tert-butoxycarbonyl-2'-methylphenyl)-2-dimethylamino-4-enoic acid (-)-8-phenylmenthol ester

: 1088481-66-6
(2R)-2-(5'-tert-butoxycarbonyl-2'-methylphenyl)-2-dimethylamino-4-enoic acid (-)-8-phenylmenthol ester

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; at -60 ℃; for 8h; diastereoselective reaction; Inert atmosphere;
DOI:10.1039/b811162f