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C34H41NO6Si

Base Information
  • Chemical Name:C34H41NO6Si
  • CAS No.:1435943-76-2
  • Molecular Formula:C34H41NO6Si
  • Molecular Weight:587.788
  • Hs Code.:
C<sub>34</sub>H<sub>41</sub>NO<sub>6</sub>Si

Synonyms:C34H41NO6Si

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Chemical Property of C34H41NO6Si
Chemical Property:
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Technology Process of C34H41NO6Si

There total 7 articles about C34H41NO6Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 ℃; for 1.5h; Inert atmosphere;
DOI:10.1002/asia.201200820
Guidance literature:
Multi-step reaction with 2 steps
1: dimethyl sulfoxide; trifluorormethanesulfonic acid / 5.5 h / 20 - 100 °C / Molecular sieve; Inert atmosphere
2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 1.5 h / 0 °C / Inert atmosphere
With dmap; trifluorormethanesulfonic acid; dimethyl sulfoxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane;
DOI:10.1002/asia.201200820
Guidance literature:
Multi-step reaction with 4 steps
1: sodium hydride / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere
2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 6 h / 0 - 20 °C / Inert atmosphere
3: dimethyl sulfoxide; trifluorormethanesulfonic acid / 5.5 h / 20 - 100 °C / Molecular sieve; Inert atmosphere
4: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 1.5 h / 0 °C / Inert atmosphere
With dmap; trifluorormethanesulfonic acid; sodium hydride; dimethyl sulfoxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; 1: |Horner-Wadsworth-Emmons Olefination;
DOI:10.1002/asia.201200820
upstream raw materials:

C24H27NO3Si

C10H16O4

hex-5-en-1-al

ethyl (2E)-2,7-octadienoate

Downstream raw materials:

C18H21NO5

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