Technology Process of C34H41NO6Si
There total 7 articles about C34H41NO6Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
dichloromethane;
at 0 ℃;
for 1.5h;
Inert atmosphere;
DOI:10.1002/asia.201200820
- Guidance literature:
-
Multi-step reaction with 2 steps
1: dimethyl sulfoxide; trifluorormethanesulfonic acid / 5.5 h / 20 - 100 °C / Molecular sieve; Inert atmosphere
2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 1.5 h / 0 °C / Inert atmosphere
With
dmap; trifluorormethanesulfonic acid; dimethyl sulfoxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
dichloromethane;
DOI:10.1002/asia.201200820
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium hydride / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere
2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 6 h / 0 - 20 °C / Inert atmosphere
3: dimethyl sulfoxide; trifluorormethanesulfonic acid / 5.5 h / 20 - 100 °C / Molecular sieve; Inert atmosphere
4: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 1.5 h / 0 °C / Inert atmosphere
With
dmap; trifluorormethanesulfonic acid; sodium hydride; dimethyl sulfoxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; dichloromethane;
1: |Horner-Wadsworth-Emmons Olefination;
DOI:10.1002/asia.201200820