Technology Process of C23H36O3Si
There total 4 articles about C23H36O3Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetra-(n-butyl)ammonium iodide; potassium hexamethylsilazane;
In
tetrahydrofuran; toluene;
at -10 ℃;
for 1h;
Inert atmosphere;
DOI:10.1016/j.tet.2013.08.026
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: methanol; pyridinium p-toluenesulfonate / 0.67 h / 20 °C / Inert atmosphere
1.2: Inert atmosphere
2.1: sodium methylate / tetrahydrofuran / 7 h / 0 °C / Inert atmosphere
3.1: methanol; pyridinium p-toluenesulfonate / 0.5 h / 20 °C / Inert atmosphere
3.2: Inert atmosphere
4.1: tetra-(n-butyl)ammonium iodide; potassium hexamethylsilazane / tetrahydrofuran; toluene / 1 h / -10 °C / Inert atmosphere
With
methanol; sodium methylate; pyridinium p-toluenesulfonate; tetra-(n-butyl)ammonium iodide; potassium hexamethylsilazane;
In
tetrahydrofuran; toluene;
DOI:10.1016/j.tet.2013.08.026
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: methanol; pyridinium p-toluenesulfonate / 0.5 h / 20 °C / Inert atmosphere
1.2: Inert atmosphere
2.1: tetra-(n-butyl)ammonium iodide; potassium hexamethylsilazane / tetrahydrofuran; toluene / 1 h / -10 °C / Inert atmosphere
With
methanol; pyridinium p-toluenesulfonate; tetra-(n-butyl)ammonium iodide; potassium hexamethylsilazane;
In
tetrahydrofuran; toluene;
DOI:10.1016/j.tet.2013.08.026
