(3,5-bis(chloromethyl)benzyl)(3-tert-butyl-5-(tritylthiomethyl)benzyl)sulfane

Base Information

Chemical Name:(3,5-bis(chloromethyl)benzyl)(3-tert-butyl-5-(tritylthiomethyl)benzyl)sulfane
CAS No.:1352833-75-0
Molecular Formula:C₄₀H₄₀Cl₂S₂
Molecular Weight:655.796
Hs Code.:

Synonyms:(3,5-bis(chloromethyl)benzyl)(3-tert-butyl-5-(tritylthiomethyl)benzyl)sulfane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3,5-bis(chloromethyl)benzyl)(3-tert-butyl-5-(tritylthiomethyl)benzyl)sulfane

Chemical Property:

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Technology Process of (3,5-bis(chloromethyl)benzyl)(3-tert-butyl-5-(tritylthiomethyl)benzyl)sulfane

There total 5 articles about (3,5-bis(chloromethyl)benzyl)(3-tert-butyl-5-(tritylthiomethyl)benzyl)sulfane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 1352833-74-9
(3-tert-butyl-5-(tritylthiomethyl)phenyl)methanethiol

: 17299-97-7
α,α',α''-trichloromesitylene

: 1352833-75-0
(3,5-bis(chloromethyl)benzyl)(3-tert-butyl-5-(tritylthiomethyl)benzyl)sulfane

Guidance literature:: With sodium hydride; In tetrahydrofuran; mineral oil; at 0 - 20 ℃; for 2h; Inert atmosphere;
DOI:10.1002/chem.201101837

Reference yield:

: 98-19-1
5-tert-Butyl-m-xylene

: 1352833-75-0
(3,5-bis(chloromethyl)benzyl)(3-tert-butyl-5-(tritylthiomethyl)benzyl)sulfane

Guidance literature:: Multi-step reaction with 4 steps

1.1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / Methyl formate / 3 h

2.1: potassium carbonate / tetrahydrofuran / 20 h / Inert atmosphere; Reflux

3.1: potassium thioacetate / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

3.2: 1 h / 20 °C / Inert atmosphere

4.1: sodium hydride / tetrahydrofuran; mineral oil / 2 h / 0 - 20 °C / Inert atmosphere

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); sodium hydride; potassium carbonate; potassium thioacetate; In tetrahydrofuran; Methyl formate; mineral oil;
DOI:10.1002/chem.201101837

Reference yield:

: 1056547-91-1
(3-(bromomethyl)-5-tert-butylbenzyl)(trityl)sulfane

: 1352833-75-0
(3,5-bis(chloromethyl)benzyl)(3-tert-butyl-5-(tritylthiomethyl)benzyl)sulfane

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium thioacetate / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

1.2: 1 h / 20 °C / Inert atmosphere

2.1: sodium hydride / tetrahydrofuran; mineral oil / 2 h / 0 - 20 °C / Inert atmosphere

With sodium hydride; potassium thioacetate; In tetrahydrofuran; mineral oil;
DOI:10.1002/chem.201101837